A rapid synthesis of isoxazolo[5,4-d]pyrimidin-4(5H)-ones under microwave irradiation with solid acid catalysis in solvent-free conditions

A. Davoodnia M. Roshani S.H. Malaeke M. Bakavoli

引用本文: A. Davoodnia,  M. Roshani,  S.H. Malaeke,  M. Bakavoli. A rapid synthesis of isoxazolo[5,4-d]pyrimidin-4(5H)-ones under microwave irradiation with solid acid catalysis in solvent-free conditions[J]. Chinese Chemical Letters, 2008, 19(5): 525-528. doi: 10.1016/j.cclet.2008.01.037 shu
Citation:  A. Davoodnia,  M. Roshani,  S.H. Malaeke,  M. Bakavoli. A rapid synthesis of isoxazolo[5,4-d]pyrimidin-4(5H)-ones under microwave irradiation with solid acid catalysis in solvent-free conditions[J]. Chinese Chemical Letters, 2008, 19(5): 525-528. doi: 10.1016/j.cclet.2008.01.037 shu

A rapid synthesis of isoxazolo[5,4-d]pyrimidin-4(5H)-ones under microwave irradiation with solid acid catalysis in solvent-free conditions

摘要: A rapid and efficient method for the synthesis of isoxazolo[5,4-d]pyrimidin-4(5H)-ones has been developed throughcyclocondensation of 5-aminoisoxazole-4-carboxamides with orthoesters under conventional heating and solvent-free microwaveirradiation with solid acid catalysis. In comparison, the reactions are faster and the yields are higher under microwave irradiation.

English

  • 加载中
计量
  • PDF下载量:  2
  • 文章访问数:  790
  • HTML全文浏览量:  1
文章相关
  • 收稿日期:  2007-12-03
通讯作者: 陈斌, bchen63@163.com
  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

  1. 本站搜索
  2. 百度学术搜索
  3. 万方数据库搜索
  4. CNKI搜索

/

返回文章