引用本文:
Xiang Wei Liao, Bao He Guan, Zhan Zhu Liu. A new and efficient method for the synthesis of isoquinoline-3-carboxylate[J]. Chinese Chemical Letters,
2008, 19(3): 253-255.
doi:
10.1016/j.cclet.2007.12.025
Citation: Xiang Wei Liao, Bao He Guan, Zhan Zhu Liu. A new and efficient method for the synthesis of isoquinoline-3-carboxylate[J]. Chinese Chemical Letters, 2008, 19(3): 253-255. doi: 10.1016/j.cclet.2007.12.025
Citation: Xiang Wei Liao, Bao He Guan, Zhan Zhu Liu. A new and efficient method for the synthesis of isoquinoline-3-carboxylate[J]. Chinese Chemical Letters, 2008, 19(3): 253-255. doi: 10.1016/j.cclet.2007.12.025
A new and efficient method for the synthesis of isoquinoline-3-carboxylate
摘要:
An isoquinoline-3-carboxylate compound 3 was obtained with a moderate yield of 40% when N-acetyl-(3'-hydroxy-4'-methoxy-5'-methyl) phenylalanine methyl ester 1 was refluxed in HMTA/TFA. However, the anticipated product N-acetyl-(3'-hydroxy-4'-methoxy-5'-methyl-6'-formyl) phenylalanine methyl ester 2 could not be found. The possible mechanism was discussed in this article.
English
A new and efficient method for the synthesis of isoquinoline-3-carboxylate
Abstract:
An isoquinoline-3-carboxylate compound 3 was obtained with a moderate yield of 40% when N-acetyl-(3'-hydroxy-4'-methoxy-5'-methyl) phenylalanine methyl ester 1 was refluxed in HMTA/TFA. However, the anticipated product N-acetyl-(3'-hydroxy-4'-methoxy-5'-methyl-6'-formyl) phenylalanine methyl ester 2 could not be found. The possible mechanism was discussed in this article.
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