双金属MOF衍生的CoZn-C/MWCNTs复合材料用于轻质宽带微波吸收

引用本文: 刘亚楠, 苏晓岗, 兰笛, 刘江涌, 马卫海, 刘亚青. 双金属MOF衍生的CoZn-C/MWCNTs复合材料用于轻质宽带微波吸收[J]. 物理化学学报, 2026, 42(6): 100276. doi: 10.1016/j.actphy.2026.100276 shu

Citation: Yanan Liu, Xiaogang Su, Di Lan, Jiangyong Liu, Weihai Ma, Yaqing Liu. Bimetallic MOF-derived CoZn-C/MWCNTs composite for lightweight and wideband microwave absorption[J]. Acta Physico-Chimica Sinica, 2026, 42(6): 100276. doi: 10.1016/j.actphy.2026.100276 shu

双金属MOF衍生的CoZn-C/MWCNTs复合材料用于轻质宽带微波吸收

刘亚楠 ^1, ,
苏晓岗 ^{1,
,} ,
兰笛 ^2, ,
刘江涌 ^1, ,
马卫海 ^{3,
,} ,
刘亚青 ^{1,
,}

1.
中北大学材料科学与工程学院, 功能高分子复合材料山西省重点实验室, 山西太原 030051;
2.
湖北汽车工业学院汽车材料学院, 湖北十堰 442002;
3.
中国电子科技集团公司第三十三研究所, 中国-白俄罗斯电磁环境效应"一带一路"联合实验室, 山西太原 030032

通讯作者: 苏晓岗,E-mail:su_xiaogang@nuc.edu.cn; 马卫海,E-mail:zblhsys@126.com; 刘亚青,E-mail:lyq@nuc.edu.cn

基金项目:
山西省1331工程高分子功能新材料重点创新团队、山西省新材料产业创新学科群、国家超级计算太原中心、山西省重点研发计划项目(202302040201007)、中国博士后科学基金(2024M764319)及陕西省人工结构功能材料与器件重点实验室基础研究基金(AFMD-KFJJ-23203)提供的资助支持。

摘要: 在现代雷达隐身和电磁兼容领域，实现兼具宽频带、强吸收、轻质和薄型特征的高性能微波吸收材料仍然是一项重大挑战。本研究提出一种简易经济的策略，利用双金属沸石咪唑酯骨架(ZIFs)衍生物制备轻质高效微波吸收剂。通过连续湿化学法合成了一系列掺有多壁碳纳米管(MWCNTs)的ZIF-8@ZIF-67前驱体，经后续热解转化为多孔双金属MOF衍生CoZn-C/MWCNTs复合材料。通过改变前驱体中Co/Zn的摩尔比，可以精确调控热解产物的成分、微观结构和电磁特性。得益于磁损耗与介电损耗的协同作用，Co/Zn比为3 : 1的复合材料在所有样品中表现出最优的衰减常数与阻抗匹配。填料负载量仅为20 wt.%，该优化复合材料在1.9 mm厚度时实现5.29 GHz的有效吸收带宽，2.0 mm厚度时最小反射损耗达−23.78 dB。雷达散射截面模拟进一步验证了其增强的散射抑制性能。本研究为宽带电磁波吸收性能的轻质MOF基复合材料设计提供了新视角。

关键词:

English

Bimetallic MOF-derived CoZn-C/MWCNTs composite for lightweight and wideband microwave absorption

Yanan Liu ^1, ,
Xiaogang Su ^{1,
,} ,
Di Lan ^2, ,
Jiangyong Liu ^1, ,
Weihai Ma ^{3,
,} ,
Yaqing Liu ^{1,
,}

1.
Shanxi Key Laboratory of Functional Polymer Composite Material, College of Materials Science and Engineering, North University of China, Taiyuan 030051, Shanxi Province, China;
2.
School of Automotive Materials, Hubei University of Automotive Technology, Shiyan 442002, Hubei Province, China;
3.
China-Belarus "Belt and Road Initiative" Joint Laboratory on Electromagnetic Environmental Effects, The 33rd Research Institute of China Electronics Technology Group Corporation, Taiyuan 030032, Shanxi Province, China

Corresponding author: Xiaogang Su, ; Weihai Ma, ; Yaqing Liu,

Received Date: 13 February 2026
Accepted Date: 02 March 2026
Revised Date: 02 March 2026

Abstract: Achieving high-performance microwave absorbers characterized by wide bandwidth, robust absorption, lightweight properties, and thin profiles remains a critical challenge within modern radar stealth and electromagnetic compatibility domains. In this study, we introduce a straightforward and cost-effective strategy for fabricating lightweight and efficient microwave absorbers utilizing composites derived from bimetallic zeolitic imidazolate frameworks (ZIFs). A variety of ZIF-8@ZIF-67 precursors incorporating multi-walled carbon nanotubes (MWCNTs) were synthesized through a sequential wet-chemical process. These precursors underwent conversion into porous bimetallic MOF-derived CoZn-C/MWCNTs composites via subsequent pyrolysis. The composition, microstructure, and electromagnetic characteristics of the pyrolyzed materials were precisely regulated by varying the Co/Zn molar ratio within the precursors. Due to the synergistic magnetic and dielectric dissipations, the 3 : 1 Co/Zn composite exhibited the best attenuation constant and impedance matching among all synthesized samples. Thus, the optimized composite provided a significant effective absorption bandwidth of 5.29 GHz at a thickness of 1.9 mm, coupled with an outstanding minimum reflection loss of −23.78 dB at 2.0 mm, even with a minimal filler loading of 20 wt.%. The enhanced scattering suppression behavior was additionally verified through radar cross-section simulation. This research provides a novel viewpoint on the rational design of lightweight MOF-based composites for broadband electromagnetic wave absorption performance.

Key words:

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沈阳化工大学材料科学与工程学院沈阳 110142

双金属MOF衍生的CoZn-C/MWCNTs复合材料用于轻质宽带微波吸收

通讯作者: 苏晓岗,E-mail:su_xiaogang@nuc.edu.cn; 马卫海,E-mail:zblhsys@126.com; 刘亚青,E-mail:lyq@nuc.edu.cn

English

Bimetallic MOF-derived CoZn-C/MWCNTs composite for lightweight and wideband microwave absorption

Corresponding author: Xiaogang Su, ; Weihai Ma, ; Yaqing Liu,

CCS Chemistry：嵌段共聚物自组装成 “三明治”二维有机材料，实现纳米级压力传感功能

CCS Chemistry：颜徐州、鲍哲南：你的皮肤可能是一片SPMs

CCS Chemistry：工作高效不疲劳，只须让催化剂动起来

CCS Chemistry：静电组装导向聚合- 聚电解质纳米凝胶量化制备新策略

CCS Chemistry：金黄色葡萄球菌醛基脱氢酶是如何识别特异性底物的？

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中国化学会秘书处

双金属MOF衍生的CoZn-C/MWCNTs复合材料用于轻质宽带微波吸收

通讯作者: 苏晓岗,E-mail:su_xiaogang@nuc.edu.cn; 马卫海,E-mail:zblhsys@126.com; 刘亚青,E-mail:lyq@nuc.edu.cn

English

Bimetallic MOF-derived CoZn-C/MWCNTs composite for lightweight and wideband microwave absorption

Corresponding author: Xiaogang Su, ; Weihai Ma, ; Yaqing Liu,

CCS Chemistry：嵌段共聚物自组装成 “三明治”二维有机材料，实现纳米级压力传感功能

CCS Chemistry：颜徐州、鲍哲南： 你的皮肤可能是一片SPMs

CCS Chemistry：工作高效不疲劳，只须让催化剂动起来

CCS Chemistry：静电组装导向聚合- 聚电解质纳米凝胶量化制备新策略

CCS Chemistry：金黄色葡萄球菌醛基脱氢酶是如何识别特异性底物的？

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