Synthesis of 3-Phenyl-6-formyl-3,4-dihydro-2H-1,3-benzoxazine

Qi Chao RAN Qiao TIAN Yi GU

引用本文: Qi Chao RAN,  Qiao TIAN,  Yi GU. Synthesis of 3-Phenyl-6-formyl-3,4-dihydro-2H-1,3-benzoxazine[J]. Chinese Chemical Letters, 2006, 17(10): 1305-1308. shu
Citation:  Qi Chao RAN,  Qiao TIAN,  Yi GU. Synthesis of 3-Phenyl-6-formyl-3,4-dihydro-2H-1,3-benzoxazine[J]. Chinese Chemical Letters, 2006, 17(10): 1305-1308. shu

Synthesis of 3-Phenyl-6-formyl-3,4-dihydro-2H-1,3-benzoxazine

  • 基金项目:

    We are grateful to the National Natural Science Foundation of China for financial support (No. 90405001).

摘要: A novel benzoxazine monomer containing aldehyde group, 3-phenyl-6-formyl-3,4-dihydro-2H-1, 3-benzoxazine (Ald-B), was synthesized via the Mannich condensation of formaldehyde, p-hydroxybenzaldehyde and aniline. Its structure was characterized by Fourier transform infrared spectroscopy (FTIR), proton nuclear magnetic resonance (1HNMR). The side reaction in the synthesis is discussed.

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  • 收稿日期:  2006-05-09
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