引用本文:
Yan Jiao, Zhi Jie Fang, Yu Hua Jiang, Bao Hui Zheng, Jie Cheng. Practical and concise synthesis of 2-oxo-3,4,5,6-tetraethoxyazepane from D-glucono-1,5-lactone[J]. Chinese Chemical Letters,
2008, 19(7): 795-796.
doi:
10.1016/j.cclet.2008.04.044
Citation: Yan Jiao, Zhi Jie Fang, Yu Hua Jiang, Bao Hui Zheng, Jie Cheng. Practical and concise synthesis of 2-oxo-3,4,5,6-tetraethoxyazepane from D-glucono-1,5-lactone[J]. Chinese Chemical Letters, 2008, 19(7): 795-796. doi: 10.1016/j.cclet.2008.04.044
Citation: Yan Jiao, Zhi Jie Fang, Yu Hua Jiang, Bao Hui Zheng, Jie Cheng. Practical and concise synthesis of 2-oxo-3,4,5,6-tetraethoxyazepane from D-glucono-1,5-lactone[J]. Chinese Chemical Letters, 2008, 19(7): 795-796. doi: 10.1016/j.cclet.2008.04.044
Practical and concise synthesis of 2-oxo-3,4,5,6-tetraethoxyazepane from D-glucono-1,5-lactone
摘要:
2-Oxo-3R,4S,5S,6S-tetraethoxyazepane was conveniently synthesized from D-glucono-1,5-lactone with a yield of 10% overall.The key step of synthetic route-reductive 1,6-cyclization was completed efficiently by using Ph3P to give the expected lactam.
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关键词:
- Azepane
- / Ph3P
- / Reduction
- / Iminosugars
- / Glucono lactone
English
Practical and concise synthesis of 2-oxo-3,4,5,6-tetraethoxyazepane from D-glucono-1,5-lactone
Abstract:
2-Oxo-3R,4S,5S,6S-tetraethoxyazepane was conveniently synthesized from D-glucono-1,5-lactone with a yield of 10% overall.The key step of synthetic route-reductive 1,6-cyclization was completed efficiently by using Ph3P to give the expected lactam.
-
Key words:
- Azepane
- / Ph3P
- / Reduction
- / Iminosugars
- / Glucono lactone
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