Citation:
DENG Xiao-Yan, PENG Hao, HE Hong-Wu. Synthesis, Characterization and X-ray Crystal Structure of 4-Fluoro-N-(2-methyl-5-((2-(p-tolyloxy)acetamido)-methyl)pyrimidin-4-yl)benzamide[J]. Chinese Journal of Structural Chemistry,
2014, 33(2): 223-227.
Synthesis, Characterization and X-ray Crystal Structure of 4-Fluoro-N-(2-methyl-5-((2-(p-tolyloxy)acetamido)-methyl)pyrimidin-4-yl)benzamide
摘要:
A new crystal of 4-fluoro-N-(2-methyl-5-((2-(p-tolyloxy)acetamido)methyl)pyrimidin-4-yl)benzamide has been prepared at room temperature and characterized by 1H NMR, 13C-NMR, IR, MS, elemental analysis and X-ray single-crystal determination. The compound crystallizes in monoclinic, space group P21/c with a=17.226(5), b=13.934(4), c=17.262(5) Å,β=92.180(5)°, V=4140(2) Å3, Dc=1.311 g/cm3, Z=8, F(000)=1712 and μ=0.095 mm-1. The molecular packing in the crystal is the result of N-H…O hydrogen bonds.
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关键词:
- X-ray crystallography
- / acetamido
- / benzamide
- / pyrimidin
English
Synthesis, Characterization and X-ray Crystal Structure of 4-Fluoro-N-(2-methyl-5-((2-(p-tolyloxy)acetamido)-methyl)pyrimidin-4-yl)benzamide
Abstract:
A new crystal of 4-fluoro-N-(2-methyl-5-((2-(p-tolyloxy)acetamido)methyl)pyrimidin-4-yl)benzamide has been prepared at room temperature and characterized by 1H NMR, 13C-NMR, IR, MS, elemental analysis and X-ray single-crystal determination. The compound crystallizes in monoclinic, space group P21/c with a=17.226(5), b=13.934(4), c=17.262(5) Å,β=92.180(5)°, V=4140(2) Å3, Dc=1.311 g/cm3, Z=8, F(000)=1712 and μ=0.095 mm-1. The molecular packing in the crystal is the result of N-H…O hydrogen bonds.
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Key words:
- X-ray crystallography
- / acetamido
- / benzamide
- / pyrimidin
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