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两个4-[(8-羟基-5-喹啉)偶氮]苯磺酸配合物的合成、结构及性质研究

罗亚楠 ,  许宪祝 ,  张潇 ,  于晓洋 ,  曲小姝

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引用本文: 罗亚楠, 许宪祝, 张潇, 于晓洋, 曲小姝. 两个4-[(8-羟基-5-喹啉)偶氮]苯磺酸配合物的合成、结构及性质研究[J]. 无机化学学报, 2013, 29(12): 2655-2665. doi: 10.3969/j.issn.1001-4861.2013.00.389 shu
Citation:  LUO Ya-Nan, XU Xian-Zhu, ZHANG Xiao, YU Xiao-Yang, QU Xiao-Shu. Syntheses, Structures and Properties of Two Coordination Polymers with 4-[(8-Hydroxy-5-quinolinyl)azo]-benzenesulfonic Acid[J]. Chinese Journal of Inorganic Chemistry, 2013, 29(12): 2655-2665. doi: 10.3969/j.issn.1001-4861.2013.00.389 shu

两个4-[(8-羟基-5-喹啉)偶氮]苯磺酸配合物的合成、结构及性质研究

  • 基金项目:

    国家973项目(No.2012CB821700)，NSFC国际合作研究项目(No.21120102034；20831002)，国家自然科学基金(No.51108122) (No.2012CB821700)，NSFC国际合作研究项目(No.21120102034；20831002)，国家自然科学基金(No.51108122)

    吉林省教育厅(No.2013-328)资助项目 (No.2013-328)

摘要: 以4-[(8-羟基-5-喹啉)偶氮]苯磺酸(H2L)为配体，采用溶剂热合成法合成了两个配合物[CuL(en)]·0.5H2O (1)和[CuL2][Cu(en)2]·2H2O (2)(en=乙二胺)，并采用单晶X-射线衍射、红外光谱、元素分析、X-射线粉末衍射和热重分析对其进行表征。化合物1和2通过氢键和π…π相互作用连接形成了三维超分子网格。此外，还研究了两个化合物的荧光性质。

English

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  • 收稿日期:  2013-02-20
  • 网络出版日期:  2013-06-27
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