引用本文:
夏静静, 张克华. 水相回流条件下N-取代吖啶二酮衍生物的合成[J]. 应用化学,
2013, 30(2): 242-244.
doi:
DOI:10.3724/SP.J.1095.2013.20086
Citation: XIA Jingjing, ZHANG Kehua. Synthesis of N-Substituted Acridinedione Derivatives in Refluxing Aqueous Phase[J]. Chinese Journal of Applied Chemistry, 2013, 30(2): 242-244. doi: DOI:10.3724/SP.J.1095.2013.20086
Citation: XIA Jingjing, ZHANG Kehua. Synthesis of N-Substituted Acridinedione Derivatives in Refluxing Aqueous Phase[J]. Chinese Journal of Applied Chemistry, 2013, 30(2): 242-244. doi: DOI:10.3724/SP.J.1095.2013.20086
水相回流条件下N-取代吖啶二酮衍生物的合成
English
Synthesis of N-Substituted Acridinedione Derivatives in Refluxing Aqueous Phase
Abstract:
Acridinedione derivatives were synthesized by refluxing aromatic aldehyde,5,5-dimethyl-1,3-cyclohexanedione and aniline/4-methyl-aniline in aqueous solutions via a multi-component one-pot condensation process.The yields of the target compounds varied from 69% to 90%.The established protocol possesses the virtues of environmental benign and high efficiency toward the preparation of acridinedione derivatives.
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Key words:
- aldehyde
- / dimedone
- / acridinedione
- / multi-component reaction
- / aqueous phase reaction
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