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5-异烟酰胺基异酞酸构筑的钕化合物的合成、晶体结构和荧光性质

陈满生 ,  许金生 ,  邓奕芳 ,  张春华 ,  邝代治 ,  聂雪

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引用本文: 陈满生, 许金生, 邓奕芳, 张春华, 邝代治, 聂雪. 5-异烟酰胺基异酞酸构筑的钕化合物的合成、晶体结构和荧光性质[J]. 无机化学学报, 2013, 29(12): 2673-2677. doi: 10.3969/j.issn.1001-4861.2013.00.390 shu
Citation:  CHEN Man-Sheng, XU Jin-Sheng, DENG Yi-Fang, ZHANG Chun-Hua, KUANG Dai-Zhi, NIE Xue. Hydrothermal Synthesis, Crystal Structure and Photoluminescent Property of Nd(Ⅲ) Complex Constructed from 5-(Isonicotinamido)-isophthalic Acid[J]. Chinese Journal of Inorganic Chemistry, 2013, 29(12): 2673-2677. doi: 10.3969/j.issn.1001-4861.2013.00.390 shu

5-异烟酰胺基异酞酸构筑的钕化合物的合成、晶体结构和荧光性质

  • 基金项目:

    湖南省自然科学基金(No.13JJ6069)，湖南省教育厅创新平台开放基金(No.11K009) (No.13JJ6069)，湖南省教育厅创新平台开放基金(No.11K009)

    湖南省科技计划重点(No.2012FJ2002)资助项目。 (No.2012FJ2002)

摘要: 由水热法合成了钕化合物[Nd(HINAIP)(INAIP)(H2O)2]n·nH2O (1)，(H2INAIP=5-异烟酰胺基异酞酸)，并进行了元素分析、IR、TG及X-射线衍射法表征。晶体结构表明：配合物1属于三斜晶系，P1空间群。配合物1是由桥联配体5-异烟酰胺基异酞酸的羧基氧连接成二维层，此二维结构被氢键拓展成三维超分子结构。荧光光谱测试结果表明配合物1具有典型稀土钕的近红外荧光特征。

English

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  • 收稿日期:  2013-05-08
  • 网络出版日期:  2013-06-19
通讯作者: 陈斌, bchen63@163.com
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