Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono(6A-N-1-(2-hydroxyl)-phenylethylimino-6A-deoxy)-β-cyclodextrin and covalently bonded silica gel

引用本文: Xiao Ping Chen, Zhi Ming Zhou, Hao Yuan, Zi Hui Meng. Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono(6^A-N-1-(2-hydroxyl)-phenylethylimino-6^A-deoxy)-β-cyclodextrin and covalently bonded silica gel[J]. Chinese Chemical Letters, 2008, 19(7): 797-800. doi: 10.1016/j.cclet.2008.04.045 shu

Citation: Xiao Ping Chen, Zhi Ming Zhou, Hao Yuan, Zi Hui Meng. Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono(6^A-N-1-(2-hydroxyl)-phenylethylimino-6^A-deoxy)-β-cyclodextrin and covalently bonded silica gel[J]. Chinese Chemical Letters, 2008, 19(7): 797-800. doi: 10.1016/j.cclet.2008.04.045 shu

Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono(6^A-N-1-(2-hydroxyl)-phenylethylimino-6^A-deoxy)-β-cyclodextrin and covalently bonded silica gel

School of Chemical Engineering and the Environment, Beijing Institute of Technology, Beijing[4_TD$DIF] 100081, China
基金项目:
Financial support from the National Natural Science Foundation of China (No.20572009) is gratefully acknowledged.

摘要: A novel chiral stationary phase (CSP) was prepared by immobilizing mono(6^A-N-1-(2-hydroxyl)-phenylethylimino-6^A-deoxy)-β-cyclodextrin onto the surface of silica gel via a longer spacer.This chiral stationary phase exhibited good enantios electivity for a variety of chiral compounds under reversed-phase conditions.

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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono(6^A-N-1-(2-hydroxyl)-phenylethylimino-6^A-deoxy)-β-cyclodextrin and covalently bonded silica gel

English

Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono(6^A-N-1-(2-hydroxyl)-phenylethylimino-6^A-deoxy)-β-cyclodextrin and covalently bonded silica gel

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通讯作者: 陈斌, bchen63@163.com

中国化学会秘书处

Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono(6A-N-1-(2-hydroxyl)-phenylethylimino-6A-deoxy)-β-cyclodextrin and covalently bonded silica gel

English

Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono(6A-N-1-(2-hydroxyl)-phenylethylimino-6A-deoxy)-β-cyclodextrin and covalently bonded silica gel

CCS Chemistry：嵌段共聚物自组装成 “三明治”二维有机材料，实现纳米级压力传感功能

CCS Chemistry：颜徐州、鲍哲南： 你的皮肤可能是一片SPMs

CCS Chemistry：工作高效不疲劳，只须让催化剂动起来

CCS Chemistry：静电组装导向聚合- 聚电解质纳米凝胶量化制备新策略

CCS Chemistry：金黄色葡萄球菌醛基脱氢酶是如何识别特异性底物的？

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通讯作者: 陈斌, bchen63@163.com

中国化学会秘书处

Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono(6^A-N-1-(2-hydroxyl)-phenylethylimino-6^A-deoxy)-β-cyclodextrin and covalently bonded silica gel

Preparation and chiral recognition of a novel chiral stationary phase for HPLC,based on mono(6^A-N-1-(2-hydroxyl)-phenylethylimino-6^A-deoxy)-β-cyclodextrin and covalently bonded silica gel

CCS Chemistry：颜徐州、鲍哲南：你的皮肤可能是一片SPMs