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Citation: LI Li, WEI Qing, GAO Sheng-Li, ZHANG Peng, SHI Qi-Zhen. Synthesis and Characterization of Co(AMP)₂Cl₂[J]. Chinese Journal of Applied Chemistry, ;2002, 19(9): 917-918. shu

Synthesis and Characterization of Co(AMP)₂Cl₂

1.
Department of Chemistry, Shaanxi Provincial Key Laboratory of Physico Inorganic Chemistry, Northwest University, Xi'an 710069

Corresponding author: GAO Sheng-Li,
Received Date: 17 January 2002
Available Online: 18 April 2002
Fund Project: 国家自然科学基金(20171036) (20171036)陕西省教育厅专项基金(HF01304) (HF01304)西北大学科研基金(00NW43)资助项目 (00NW43)

2-Amino-4,6-dimethoxypyrimidine(AMP) was synthesized using benzyltriethyl ammonium chloride(BTEA) as a catalyst in yield of 87.5%. A solid complex Co(AMP)₂Cl₂ was obtained by refluxing AMP with CoCl₂ in ethanol. The composition of the complex was determined by chemical and elemental analyses. The structure of the complex and sp³ d² of the hybridization type of Co²⁺ were estimated by IR, XPS and ¹H NMR.
- cobalt chloride,
- amino dimethoxypyrimidine,
- synthesis
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Synthesis and Characterization of Co(AMP)₂Cl₂