引用本文:
乔艳红, 郁铭, 孙命, 缪方明. 邻香兰素甲硫氨酸席夫碱四核铜配合物的合成及结构表征[J]. 应用化学,
2003, 20(2): 192-194.
Citation: QIAO Yan-Hong, YU Ming, SUN Ming, MIAO Fang-Ming. Synthesis and Characterization of Tetranuclear Copper Complex of O-Vanillin-Methionine[J]. Chinese Journal of Applied Chemistry, 2003, 20(2): 192-194.
Citation: QIAO Yan-Hong, YU Ming, SUN Ming, MIAO Fang-Ming. Synthesis and Characterization of Tetranuclear Copper Complex of O-Vanillin-Methionine[J]. Chinese Journal of Applied Chemistry, 2003, 20(2): 192-194.
邻香兰素甲硫氨酸席夫碱四核铜配合物的合成及结构表征
English
Synthesis and Characterization of Tetranuclear Copper Complex of O-Vanillin-Methionine
Abstract:
An O-Vanillin-methionine Schiff Base complex with copper(Ⅱ) has been synthesized under a mild condition. The complex has been characterized by elemental analysis, UV, FT-IR, TG-DTA and XRD. The crystal structure of the complex belongs to monoclinic, with space group C2/C, a=2.070 4(12) nm, b=1.431 9(8) nm, c=2.812 9(11) nm, β=133.15(2)°, V=6.084(5) nm3, Z=8, Dc=0.998 Mg/m3, F(000)=1 836, final R=0.121 8. The results revealed it is a tetranuclear copper(Ⅱ) complex.
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Key words:
- vanillin
- / methionine
- / Schiff Base
- / tetranuclear copper(Ⅱ) complex
- / synthesis
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