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Citation: ZHOU Li-Qun, LIU Shi-Zhong, YU Guo-Feng. Preparation and Properties of the Molybdovanadophosphate Nanoparticles with Dawson Structure by Solid-state Reaction[J]. Chinese Journal of Applied Chemistry, ;2003, 20(5): 479-482. shu

Preparation and Properties of the Molybdovanadophosphate Nanoparticles with Dawson Structure by Solid-state Reaction

1.
a Faculty of Chemistry and Material Science, Hubei University, Wuhan 430062;
2.
b Department of Chemistry, Xiaogan College, Xiaogan

Corresponding author: ZHOU Li-Qun,
Received Date: 4 December 2002
Available Online: 26 February 2003
Fund Project: 湖北省教育厅重大科研项目(2000Z01009) (2000Z01009)

The molybdovanadophosphate nanoparticles with Dawson structure (NH₄)₈P₂Mo₁₆V₂O₆₂·7H₂O were synthesized by solid-state reaction at room temperature and characterized by elemental analysis,IR,XRD,TEM,TG-DTA and BET techniques.The nanoparticles are found still to exhibite Dawson structure with average size being 22 nm and BET area 167 m²/g.They are stable at temperature<441℃.
- molybdovanadophosphate,
- solid-state synthesis,
- nanoparticle,
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