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Citation: CH EN Ji-Zhi, JIAO Qing-Ze, TIAN Zhou-Ling. Improvement of the Method for Nanometer PbCO₃ Powders Preparation[J]. Chinese Journal of Applied Chemistry, ;2004, 21(9): 962-965. shu

Improvement of the Method for Nanometer PbCO₃ Powders Preparation

1.
College of Chemistry and Environmental Science, Beijing Institute and Technology University, Beijing 100081

Corresponding author: JIAO Qing-Ze,
Received Date: 20 December 2003
Available Online: 27 May 2004

The structural and morphological investigations of the products PbCO₃ by common preparation method showed that the PbCO₃ crystal grows very quickly and nanometer PbCO₃ could hardly be obtained. The nanometer PbCO₃ was synthesized by mixed Pb(CH₃COO)₂·3H₂O and Na₂CO₃ in 8 000 r/min quick mixing equipment. The influences of material and concentration of reactant on the preparation of nanometer PbCO₃ were discussed. The nanoparticles as prepared showed narrow size distribution and the particle sizes of PbCO₃ were about 10~30 nm when Pb(NO₃)₂ was replaced by Pb(CH₃COO)₂·3H₂O as raw material, and the particle sizes of PbCO₃ decreased with increasing the concentration of Pb(CH₃COO)₂·3H₂O.
- nanometer PbCO₃,
- preparation,
- precipitation method
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通讯作者: 陈斌, bchen63@163.com

Improvement of the Method for Nanometer PbCO₃ Powders Preparation