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Citation: YANG Fa-Fu, CHEN Xi-Lei, LIN Jian-Rong, CAI Xiu-Qin. Synthesis and Adsorption Properties of Calix[6]-1,4-crown-amides-based Polymers[J]. Chinese Journal of Applied Chemistry, ;2004, 21(10): 1066-1068. shu

Synthesis and Adsorption Properties of Calix[6]-1,4-crown-amides-based Polymers

1.
Department of Chemistry, Fujian Normal University, Fuzhou 350007

Corresponding author: YANG Fa-Fu,
Received Date: 11 July 2003
Available Online: 23 February 2004
Fund Project: 福建省自然科学基金(E0220002) (E0220002)福建省青年科技人才创新资金(2001J025)资助项目 (2001J025)

A series of calix[6]-1,4-crown-based polymers with stable conformations were synthesized by reacting calix[6]-1,4-crown tetraester with poly(ethyleneimine), and their adsorption capabilities were studied. Their structures and shapes were characterized by elemental analyses, IR and SEM techniques. Their adsorption selectivities were found to be higher than that of calix[6] arene polymer without stable conformation. All of them showed good selective adsorption capability towards Cu²⁺ among the tested cations. The adsorption capacity of compound 2a towards Cu²⁺ at concentration of 0.2 mmol/L were 64.5×10^-5 mol/mg.
- polymeric calix[6] arene,
- stable conformation,
- adsorption capacity
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