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Citation: ZHOU Li-Qun, YANG Nian-Hua, ZHOU Li-Rong, SUN Ju-Tang. Preparation and Formation Mechanism of NiO Nanoparticles by Solid State Reaction[J]. Chinese Journal of Applied Chemistry, ;2006, 23(6): 682-684. shu

Preparation and Formation Mechanism of NiO Nanoparticles by Solid State Reaction

1.
a College of Chemistry and Molecular Science, Wuhan University, Wuhan 430072;
2.
b Faculty of Chemistry and Material Science, Hubei University, Wuhan

Corresponding author: SUN Ju-Tang,
Received Date: 19 August 2005
Available Online: 20 April 2006
Fund Project: 国家自然科学基金(20471044) (20471044)湖北省自然科学基金(2005ABA059)资助项目 (2005ABA059)

NiO nanoparticles were successfully prepared by solid state thermal decomposition of NiCO₃ (10 nm) precursor,which was synthesized by solid state reaction at room temperature.The crystal structure,particle-size and properties of the nanoparticles were characterized by means of XRD,TEM TG-DTA and BET.The results show that the NiO had an average particle size of 5.8 nm and highest BET specific surface area of 116.6 m²/g after annealling the precursor at 300℃ for 2 h.The formation mechanism of the nanoparticles were also discussed.
- NiO,
- nanoparticle,
- solid state reaction,
- synthesis mechanism
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