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Citation: SHEN Shui-Fa, LI Chang-Qing, PAN Hai-Bo, ZHENG Chun-Ming, CHEN Nai-Sheng. Preparation and Characterization of Nano Bi₂Sn₂O₇ via Water/Oil Microemulsion[J]. Chinese Journal of Applied Chemistry, ;2006, 23(6): 641-645. shu

Preparation and Characterization of Nano Bi₂Sn₂O₇ via Water/Oil Microemulsion

1.
a College of Chemistry and Chemical Engineering, Institute of Functional Materials;
2.
b Central Laboratory, Fuzhou University, Fuzhou

Corresponding author: CHEN Nai-Sheng,
Received Date: 18 July 2005
Available Online: 14 November 2005
Fund Project: 福建省教育厅(K02011) (K02011)福州大学科技发展基金(XKJ(YM)-0101)资助项目 (XKJ(YM)-0101)

The precursor of bismuth stannate(Bi₂Sn₂O₇) was prepared by precipitation reaction in the nanodroplets of water/TX100/n-hexanol/cyclohexane microemulsion system.Some factors that affected the size and shape of the precursor were investigated.Spherical bismuth stannate particles with single pyrochlore structure were obtained when the precursor was calcined at a temperature as low as 500℃.The particle size was in the range of 10~20 nm with a mean size close to 10 nm.The IR bands were broadened when calcined at 500℃.
- nanoparticles,
- Bi₂Sn₂O₇,
- microemulsion method
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Preparation and Characterization of Nano Bi₂Sn₂O₇ via Water/Oil Microemulsion