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Citation: XU Guo-Rong, REN Feng-Lian, SI Shi-Hui, YI Qing-Feng. Deposition of Nickel Nanowires in Porous Anodic Alumina Template by Direct Current Method[J]. Chinese Journal of Applied Chemistry, ;2006, 23(8): 830-834. shu

Deposition of Nickel Nanowires in Porous Anodic Alumina Template by Direct Current Method

1.
a College of Chemistry and Chemical Engineering, Central South University, Changsha 410083;
2.
b College of Chemistry and Chemical Engineering, Hunan University of Science and Technology, Xiangtan

Corresponding author: XU Guo-Rong,
Received Date: 8 October 2005
Available Online: 10 March 2006
Fund Project: 国家自然科学基金资助项目(20475065) (20475065)

A new method is presented for nickel nanowire deposition in porous anodic alumina(PAA) template by direct current.The barrier layer of PAA was removed by electrolysis in neutral potassium chloride solution with the PAA as the cathode.The electrochemical behavior of Nickel ion and hydrogen ion on PAA was studied by measuring the polarization curves.The morphology and the crystal structure of the PAA and the nickel nanowires were characterized by SEM and XRD.The cyclic voltammogram of the PAA with the barrier layer eroded showed an oxidation peak in the first scan in a 0.5 mol/L phosphate buffer solution.The deposition potential of nickel ions on PAA was -1.0 V versus Ag/AgCl.The diameter of the nanowires was about 70~80 nm based on SEM.XRD showed that the deposited material was cubic nickel orienting along the (111) direction.After the barrier layer was eroded,PAA could be used directly as a template to fabricate nickel nanowire by direct current method.
- porous anodic alumina,
- nickel nanowire,
- electrodeposition
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