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Citation: LIU Hui, LIU Lian, ZHANG Chun-Qing. Synthesis and Application of a Novel Adhesive Monomer[J]. Chinese Journal of Applied Chemistry, ;2006, 23(11): 1264-1268. shu

Synthesis and Application of a Novel Adhesive Monomer

1.
a Dalian University of Technology, Dalian;
2.
b Dalian Maritime University, Dalian 116026

Corresponding author: LIU Lian,
Received Date: 16 November 2005
Available Online: 9 April 2006
Fund Project: 辽宁省自然科学基金项目(20032124) (20032124)

10-Methacryloyloxydecyl-2-thiouracil-5-carboxylate was synthesized from the reaction of thiouracil with diethyl ethoxymethylene malonate and ω-hydroxy-decyl-methacrylate.The structure of the product was characterized by ¹H NMR,MS and FT-IR,and the effect of this product on the bond durability between composite resin with Au alloy,Ti alloy or Co-Cr alloy was evaluated.The product significantly elevated the bonding strength between composite resin and Au alloy,and the shear strength was 22.4 MPa when the mass fraction of this product was 0.5%.But this product could not enhance the bonding strength of the composite resin with Ti alloy and Co-Cr alloy;the shear strength was 12.1 MPa,13.7 MPa respectively.
- methacryloyloxydecyl-thiouracil-carboxylate,
- adhesive monomer,
- composite resin,
- dental alloy,
- bond durability
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