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Citation: JIANG Xiao-Ying, LI Xiao-Bo, LI Jian-Ping. Syntheses and Characterization of N,N'-diaryl adipyl dihydrazides[J]. Chinese Journal of Applied Chemistry, ;2007, 24(4): 465-467. shu

Syntheses and Characterization of N,N'-diaryl adipyl dihydrazides

1.
a Henan Institue of Science and Technology, Xinxiang 453003;
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b College of Chemistry & Enviromental Science, Henan Normal University, Xinxiang 453007

Corresponding author: JIANG Xiao-Ying,
Received Date: 4 May 2006
Available Online: 25 July 2006
Fund Project: 河南省自然科学基金(0111010680)资助项目 (0111010680)

Synthesis of a series of N,N'-diaryl adipyl dihydrazide compounds from self-made adipic chloride and substituted phenylhydrazine were reported.Nine kinds of compounds was synthesized using the method of ice bathing.The products were confirmed by means of elemental analysis,IR and ¹H NMR.Two N-H absorptions of products were observed at approximately 3 200~3 400 cm^-1 in the infrared spectrum.Resonances corresponding to the N-H chemical shift were from 7.3 to 10.5 in ¹H NMR.The results of elemental analysis for the products were in agreement with the theoretical values.The yields were about from 81% to 93%.
- adipic chloride,
- substituted benzyldiazane,
- N,N'-diaryl adipyl dihydrazide,
- synthesis
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