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Citation: YAN Jing-Hui, LI Zhong-Tian, ZHANG Hai-Yan, WANG Lin-Kun, CAO Liang-Jun, Qi Yun-Yun, SHI Chun-Shan. Synthesis and Fluorescence of BaYF₅:Ce³⁺ Nanoparticles[J]. Chinese Journal of Applied Chemistry, ;2008, 25(2): 254-256. shu

Synthesis and Fluorescence of BaYF₅:Ce³⁺ Nanoparticles

1.
a College of Chemistry and Environmental Engineering, Changchun University of Science and Technology, Changchun 130022;
2.
b Key Laboratory of Rare Earth Chemistry and Physics, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun

Corresponding author: YAN Jing-Hui,
Received Date: 22 February 2007
Available Online: 11 July 2007
Fund Project: 吉林省科技厅基金(20050507) (20050507)长春市科技局基金(2005093)资助项目 (2005093)

BaYF₅:Ce³⁺ nanoparticles were synthesized from the quaternary water/CTAB/bulanol/octane microemulsion system.The complex fluorides were characterzed by means of X-ray powder diffraction(XRD),environmental scanning electron microscopy(ESEM) and fluorescence spectrometry.XRD analysis shows that the products are in accord with the standard JCPDS card NO.18-715,the products are single phase and the crystal structure of BaYF₅:Ce³⁺ particles is not changed obviously.The average grain size of the products is about 20 nm obtained from the ESEM.The fluorescence of BaYF₅:Ce³⁺ particles was observed.The emission peak located at 330 nm is attributed to the d→f transition of Ce³⁺.Compared with those of the powder crystal prepared by high temperature solid reaction,the emission peaks of the fluorescent spectra showed a blue shift of 5 nm.
- BaYF₅:Ce³⁺,
- nanoparticle,
- microemulsion
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Synthesis and Fluorescence of BaYF₅:Ce³⁺ Nanoparticles