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Citation: HU Ai-Xi, MA Ying-Qi, XIA Lin, YU Zheng-Ying. Synthesis and Characterization of 4-(6-Methoxynaphthalen-2-yl)-2-Benzyliminothiazole[J]. Chinese Journal of Applied Chemistry, ;2008, 25(8): 966-970. shu

Synthesis and Characterization of 4-(6-Methoxynaphthalen-2-yl)-2-Benzyliminothiazole

HU Ai-Xi ^a,, ,
MA Ying-Qi ^b ,
XIA Lin ^a ,
YU Zheng-Ying ^a

1.
a College of Chemistry and Chemical Engineering, Hunan University, Changsha 410082;
2.
b School of Chemical and Energy Engineering, South China University of Technology, Guangzhou

Corresponding author: HU Ai-Xi,
Received Date: 23 July 2007
Available Online: 30 September 2007

4-(6-Methoxynaphthalen-2-yl)thiazol-2-amine was first prepared from 2-bromo-1-(6-methoxy-naphthalen-2-yl)alkyl-1-one and thiourea. 4-(6-Methoxynaphthalen-2-yl)-2-benzylimino-thiazole was then synthesized via the reaction of 4-(6-methoxynaphthalen-2-yl)thiazol-2-amine with salicylal with yields of 72.1%~94.8%. The structures of the compounds were determined by ¹H NMR, IR and elemental analysis. Proton assiqnment of naphthyl was performed by analyzing coupling constants of the protons on the naphthyl of target compound and intermediate.
- (methoxynaphthalenyl) benzyliminothiazole,
- synthesis,
- characterization
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