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Citation: LIU Chun-Xia, HOU Wan-Guo. Synthesis of Hydrotalcite-like Compound with Uniform Size[J]. Chinese Journal of Applied Chemistry, ;2008, 25(8): 882-885. shu

Synthesis of Hydrotalcite-like Compound with Uniform Size

LIU Chun-Xia ^a ,
HOU Wan-Guo ^a,b,,

1.
a Key Laboratory for Colloid and Interface Chemistry of State Education Ministry, Shandong University, Ji'nan;
2.
b Engineering research Center for Colloid Materials of Shandong Province, Shandong University, Ji'nan 250100

Corresponding author: HOU Wan-Guo,
Received Date: 22 August 2007
Available Online: 17 December 2007
Fund Project: 国家重大基础研究(九七三)计划(2004CB418504) (九七三)计划(2004CB418504)国家自然科学基金(20573065) (20573065)山东省自然科学基金(Z2005B02)项目 (Z2005B02)

Mg-Al hydrotalcite-like compound(HTlc) was synthesized by the co-precipitation method, and the effects of temperature(T), aging time (t), total metal ion concentration(c) and mixing method on the size and size distribution of HTlc were investigated by orthogonal design method. It was found that the primary factor affecting the size of Mg-Al HTlc was aging time, while that affecting the size distribution of Mg-Al HTlc was mixing method. The optimal synthesis method and conditions for Mg-Al HTlc with small uniform size were obtained: decreasing pH method, T=25℃, c=0.50 mol/L and t=0.75 h.
- hydrotalcite-like compounds,
- mean size,
- size distribution,
- layered double hydroxides,
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