Citation: LUO Ya-Nan, XU Xian-Zhu, ZHANG Xiao, YU Xiao-Yang, QU Xiao-Shu. Syntheses, Structures and Properties of Two Coordination Polymers with 4-[(8-Hydroxy-5-quinolinyl)azo]-benzenesulfonic Acid[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(12): 2655-2665. doi: 10.3969/j.issn.1001-4861.2013.00.389 shu

Syntheses, Structures and Properties of Two Coordination Polymers with 4-[(8-Hydroxy-5-quinolinyl)azo]-benzenesulfonic Acid

1.
1 State Key Laboratory of Urban Water Resource and Environment, Harbin Institute of Technology, Harbin 150080, China;

Received Date: 20 February 2013
Available Online: 27 June 2013
Fund Project: 国家973项目(No.2012CB821700)，NSFC国际合作研究项目(No.21120102034；20831002)，国家自然科学基金(No.51108122) (No.2012CB821700)，NSFC国际合作研究项目(No.21120102034；20831002)，国家自然科学基金(No.51108122)吉林省教育厅(No.2013-328)资助项目 (No.2013-328)

Two coordination polymers based on 4-[(8-hydroxy-5-quinolinyl)azo]-benzenesulfonic acid(H₂L), namely [CuL(en)]·0.5H₂O (1) and [CuL₂][Cu(en)₂]·2H₂O (2)(en=ethylenediamine) have been solvothermally synthesized and structurally characterized by single-crystal X-ray diffraction, infrared (IR) spectra, elemental analysis, powder X-ray diffractions (PXRD) and thermogravimetric analysis (TGA). compounds 1 and 2 are connected into three-dimensional (3D) supramolecular networks by both hydrogen bonding and π…π interactions. In addition, their fluorescent properties have been investigated. CCDC: 881778, 1; 889463, 2.
- three-dimensional supramolecular network;4-[(8-hydroxy-5-quinolinyl)azo]-benzenesulfonic acid;solvothermal synthesis;fluorescent property
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沈阳化工大学材料科学与工程学院沈阳 110142