Citation: LIU Dao-Sen, LIANG Fa-Ku, WANG Zhi-Wu. Synthesis, Structure and Luminescence of a 1D Zinc(Ⅱ) Coordination Polymer Constructed from 4’-Hydroxyl-biphenyl-4-carboxylate and 1,3-Bis(4-pyridyl)propane Ligands[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(9): 2007-2012. doi: 10.3969/j.issn.1001-4861.2013.00.262 shu

Synthesis, Structure and Luminescence of a 1D Zinc(Ⅱ) Coordination Polymer Constructed from 4’-Hydroxyl-biphenyl-4-carboxylate and 1,3-Bis(4-pyridyl)propane Ligands

1.
1 Communication and Electronic Engineering Institute, Qiqihar University, Qiqihar, Heilongjiang 161006, China;

Received Date: 19 January 2013
Available Online: 25 March 2013
Fund Project: 齐齐哈尔大学青年教师科研启动基金(No．2011K-M07)资助项目。 (No．2011K-M07)

A new 1D zinc(Ⅱ) coordination polymer {[Zn(Hhbc)₂(bpp)]H₂O}_n (1) (Hhbc=4'-Hydroxyl-biphenyl-4-carboxylate, bpp=1,3-bis(4-pyridyl)propane) has been synthesized by hydrothermal method and characterized by elemental analysis, IR, TGA, powder X-ray diffraction and single-crystal X-ray diffraction. The carboxylate oxygens of two different Hhbc ligands connect one Zn^Ⅱ ion in bidentate-chelating and monodentate coordinated modes to form mononuclear zinc building blocks, which are further linked into a 1D infinite chain through trans-bpp ligands. These chains are further linked into a 2D supramolecular network through water-hydroxyl tetramers involving the free water molecules and hydroxyl groups of Hhbc ligands. Furthermore, the luminescent property of complex 1 was investigated at room temperature. CCDC: 919045.
- zinc(Ⅱ) coordination polymer;hydrothermal synthesis;crystal structure;luminescence
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沈阳化工大学材料科学与工程学院沈阳 110142