Citation: GUO Bing-Zhi, ZHAO Yun, LI Han-Sheng, JIAO Qing-Ze. Preparation and Characterization of Amino-functionalized Multi-walled Carbon Nanotubes[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(9): 1825-1829. doi: 10.3969/j.issn.1001-4861.2013.00.194 shu

Preparation and Characterization of Amino-functionalized Multi-walled Carbon Nanotubes

1.
1 School of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing 100081, China;

Received Date: 6 January 2012
Available Online: 12 March 2013
Fund Project: 国家自然科学基金(No.21071017)资助项目。 (No.21071017)

Cyano functional groups were covalently attached to the surface of multi-walled carbon nanotubes(MWNTs) by free radical addition of AIBN, then Al-NiCl₂·6H₂O-THF system was used to reduce the cyano to obtain amino-functionalized carbon nanotubes. The structure and morphology of amino-functionalized MWNTs were characterized by Raman spectroscopy, thermal gravimetric analysis, X-ray photoelectron spectroscopy and transmission electron microscopy. The results showed that amino group was linked to the surface of MWNTs and approximately 17.1 of every 1 000 carbon atoms on the surface of MWNTs were grafted to amino groups.
- carbon nanotubes;functionalization;amino;Al-NiCl₂·6H₂O-THF
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沈阳化工大学材料科学与工程学院沈阳 110142