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Citation: ZHUO Na, LI Li, GAO Yu, LU Lu, HUANG Xian-Dan, WANG Li-Li. CTAB-Assisted Synthesis of Nano-Composite Ag/ZnO-TiO2 and Its UV Photocatalytic Activity[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(5): 991-998. doi: 10.3969/j.issn.1001-4861.2013.00.156 shu

CTAB-Assisted Synthesis of Nano-Composite Ag/ZnO-TiO2 and Its UV Photocatalytic Activity

  • 1.

    Faculty of Chemistry and Chemical Engineering, Qiqihar University, Qiqihar, Helongjiang 161006, China

  • Corresponding author: LI Li, 
  • Received Date: 25 December 2012
    Available Online: 1 February 2013

    Fund Project: 黑龙江省自然科学基金 (No.B201106) (No.B201106)黑龙江省教育厅科学技术项目(No.12511592) (No.12511592)黑龙江省政府博士后资助经费(No.LBH-Z11108) (No.LBH-Z11108) 黑龙江省研究生创新科研项目(No.YJSCX2011-199HLJ) (No.YJSCX2011-199HLJ)齐齐哈尔大学研究生创新科研项目(No.YJSCX2010-017X)资助项目。 (No.YJSCX2010-017X)

  • The nano-composites Ag/ZnO-TiO2 under cetyltrimethylammonium bromide(CTAB) were prepared with molar ratio of 0.1:2:1 about Ag:Zn:Ti by the sol-gel method combined with temperature-programmed treatment. The phase composition, structures and morphologies of the nano-composite Ag/ZnO-TiO2 by post-processing methods of calcination at different temperature(500, 600, 700 ℃) and time(5 h, 7 h) were well-characterized by X-ray diffraction(XRD), and UV-visible diffuse reflectance spectrometer(UV-Vis/DRS), and X-ray photoelectron spectroscopy(XPS), and Transmission electron microscopy(TEM), and Scanning electron microscopy combined with X-ray energy dispersive spectroscopy(SEM-EDS) and N2 adsorption-desorption measurement. Results showed that a series of composites had not only the ZnO wurtzite and TiO2 anatase structures, meanwhile, part Zn2TiO4 were generated and silver species existing in the nano-composite Ag/ZnO-TiO2 was metallic Ag0. By the method changed calcination temperature and time, different nano-composites Ag/ZnO-TiO2(CTAB) showed nanowires and nano-ball morphology, moreover, which were uniformly distribution. By the photocatalytic degradation of RB, under UV light irradiation, the results showed that the activities of sample calcined at different time and temperature were obvious distinction.
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    1. [1]

      [1] Yang X, Xu L L, Yu X D, et al. Catal. Commun., 2008,9(6): 1224-1229

    2. [2]

      [2] Chen F, Zou W W, Qu W W, et al. Catal. Commun., 2009,10 (11):1510-1513

    3. [3]

      [3] Yang X, Wang Y H, Xu L L, et al. J. Phys. Chem. C, 2008, 112(30):11481-11489

    4. [4]

      [4] LI Li(李莉), LU Dan(陆丹), ZHAO Yue-Hong(赵月红), et al. Chinese J. Inorg. Chem. (Wuji Huaxue Xuebao), 2011,27(3): 451-456

    5. [5]

      [5] Guo G M, Yu B B, Yu P, et al. Talanta, 2009,79(3):570-575

    6. [6]

      [6] Wang C H, Shao C L, Zhang X T, et al. Inorg. Chem., 2009, 48(15):7261-7268

    7. [7]

      [7] Wang J, Li J, Zhang L Q, et al. Catal. Lett., 2009,130(3/4): 551-557

    8. [8]

      [8] LI Li(李莉), MA Yu(马禹), CAO Yan-Zhen(曹艳珍), et al. Acta Phys.-Chim. Sin.(Wuli Huaxue Xuebao), 2009,25(7): 1461-1466

    9. [9]

      [9] He Z Y, Li Y G, Zhang Q G, et al. Appl. Catal. B, 2010,93 (3/4): 376-382

    10. [10]

      [10] Xu L, Steinmiller E M P, Skrabalak S E. J. Phys. Chem. C, 2010,116(1):871-877

    11. [11]

      [11] Chen D, Zhang H, Hu S, et al. J. Phys. Chem. C, 2008,112 (1):117-122

    12. [12]

      [12] Lin D D, Hui W, Zhang R, et al. J. Chem. Mater., 2009,21 (15):3479-3484

    13. [13]

      [13] Lu W W, Gao S Y, Wang J J. J. Phys. Chem. C, 2008,112 (43):16792-16800

    14. [14]

      [14] Kuai L, Geng B Y, Chen X T, et al. Langmuir., 2010,26(24): 18723-18727

    15. [15]

      [15] Yang Z J, Lv L L, Dai Y L, et al. Appl. Surf. Sci., 2010,256 (9):2898-2902

    16. [16]

      [16] Yang Y Q, Du G H, Xin X, et al. Appl. Phys. A, 2011,104 (4):1229-1235

    17. [17]

      [17] LI Li(李莉), ZHUO Na(禚娜), GAO Yu(高宇), et al. Chem. J. Chinese Universities(Gaodeng XueXiao Huaxue Xuebao), 2012,33(6):1264-1270

    18. [18]

      [18] Zhang H, Wang G, Chen D, et al. Chem. Mater., 2008,20 (20):6543-6549

    19. [19]

      [19] Sasaoka E, Sada N, Manabe A, et al. Ind. Eng. Chem. Res., 1999,38(3):958-963

    20. [20]

      [20] Nolan N T, Seery M K, Pillai S C. Chem. Mater., 2011,23(6): 1496-1504

    21. [21]

      [21] Liu R L, Huang Y X, Xiao A H, et al. J. Alloys Compd., 2010,503(1):103-110

    22. [22]

      [22] Wang T, Jiang X, Mao C W. Langmuir, 2008,24(24):14042- 14047

    23. [23]

      [23] Sun T J, Qiu J S, Liang C H. J. Phys. Chem. C, 2008,112 (3):715-721

    24. [24]

      [24] Ou H H, Lo S L, Liao C H. J. Phys. Chem. C, 2011,115 (10):4000-4007

    25. [25]

      [25] Wu T S, Wang K X, Li G D, et al. ACS. Appl Mater&Inter., 2010,2(2):544-550

    26. [26]

      [26] Moulder J F, Stick W F, Sobol P E, et al. Handbook of X- ray Photoelectron Spectroscopy [M] . Eden Prairie: Perkin- Elmer. Corp, 1992:pp182183

    27. [27]

      [27] Ren W, Ai Z, Jia F, et al. Appl. Catal. B, 2007,69(3/4):138- 144

    28. [28]

      [28] Xin B F, Jing L Q, Ren Z Y, et al. J. Phys. Chem. B, 2005, 109(7):2805-2809

    29. [29]

      [29] Poyraz A S, Dag O. J. Phys. Chem. C, 2009,113(43):18596- 18607

    30. [30]

      [30] Sing K S W, Everett D H, Haul R A W. Pure. Appl. Chem., 1985,57(4):603-619

    31. [31]

      [31] ZOU Wen(邹文), HAO Wei-Chang(郝维昌), XIN Xin(信心), et al. Chinese J. Inorg. Chem. (Wuji Huaxue Xuebao), 2009, 25(11):1971-1976

    32. [32]

      [32] Wen Z H, Wang G, Lu W, et al. Cryst. Growth Des., 2007,7 (9):1722-1725

    33. [33]

      [33] Sudeep P K, Kamat P V. Chem. Mater., 2010,17(22):5404- 5410

    34. [34]

      [34] Gu C D, Cheng C C, Huang H Y, et al. Cryst. Growth Des., 2009,9(7):3278-3285

    35. [35]

      [35] Ldgar M, Jancar B, Sturm S, et al. Langmuir, 2010,26(14): 12215-12224

    36. [36]

      [36] Lei Y Z, Zhao G H, Liu M C, et al. J. Phys. Chem. C, 2009, 113(44):19067-19076

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