Advanced Search

Citation: ZHUO Na, LI Li, GAO Yu, LU Lu, HUANG Xian-Dan, WANG Li-Li. CTAB-Assisted Synthesis of Nano-Composite Ag/ZnO-TiO2 and Its UV Photocatalytic Activity[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(5): 991-998. doi: 10.3969/j.issn.1001-4861.2013.00.156 shu

CTAB-Assisted Synthesis of Nano-Composite Ag/ZnO-TiO2 and Its UV Photocatalytic Activity

  • 1.

    Faculty of Chemistry and Chemical Engineering, Qiqihar University, Qiqihar, Helongjiang 161006, China

  • Corresponding author: LI Li, 
  • Received Date: 25 December 2012
    Available Online: 1 February 2013

    Fund Project: 黑龙江省自然科学基金 (No.B201106) (No.B201106)黑龙江省教育厅科学技术项目(No.12511592) (No.12511592)黑龙江省政府博士后资助经费(No.LBH-Z11108) (No.LBH-Z11108) 黑龙江省研究生创新科研项目(No.YJSCX2011-199HLJ) (No.YJSCX2011-199HLJ)齐齐哈尔大学研究生创新科研项目(No.YJSCX2010-017X)资助项目。 (No.YJSCX2010-017X)

  • The nano-composites Ag/ZnO-TiO2 under cetyltrimethylammonium bromide(CTAB) were prepared with molar ratio of 0.1:2:1 about Ag:Zn:Ti by the sol-gel method combined with temperature-programmed treatment. The phase composition, structures and morphologies of the nano-composite Ag/ZnO-TiO2 by post-processing methods of calcination at different temperature(500, 600, 700 ℃) and time(5 h, 7 h) were well-characterized by X-ray diffraction(XRD), and UV-visible diffuse reflectance spectrometer(UV-Vis/DRS), and X-ray photoelectron spectroscopy(XPS), and Transmission electron microscopy(TEM), and Scanning electron microscopy combined with X-ray energy dispersive spectroscopy(SEM-EDS) and N2 adsorption-desorption measurement. Results showed that a series of composites had not only the ZnO wurtzite and TiO2 anatase structures, meanwhile, part Zn2TiO4 were generated and silver species existing in the nano-composite Ag/ZnO-TiO2 was metallic Ag0. By the method changed calcination temperature and time, different nano-composites Ag/ZnO-TiO2(CTAB) showed nanowires and nano-ball morphology, moreover, which were uniformly distribution. By the photocatalytic degradation of RB, under UV light irradiation, the results showed that the activities of sample calcined at different time and temperature were obvious distinction.
  • 加载中
    1. [1]

      [1] Yang X, Xu L L, Yu X D, et al. Catal. Commun., 2008,9(6): 1224-1229

    2. [2]

      [2] Chen F, Zou W W, Qu W W, et al. Catal. Commun., 2009,10 (11):1510-1513

    3. [3]

      [3] Yang X, Wang Y H, Xu L L, et al. J. Phys. Chem. C, 2008, 112(30):11481-11489

    4. [4]

      [4] LI Li(李莉), LU Dan(陆丹), ZHAO Yue-Hong(赵月红), et al. Chinese J. Inorg. Chem. (Wuji Huaxue Xuebao), 2011,27(3): 451-456

    5. [5]

      [5] Guo G M, Yu B B, Yu P, et al. Talanta, 2009,79(3):570-575

    6. [6]

      [6] Wang C H, Shao C L, Zhang X T, et al. Inorg. Chem., 2009, 48(15):7261-7268

    7. [7]

      [7] Wang J, Li J, Zhang L Q, et al. Catal. Lett., 2009,130(3/4): 551-557

    8. [8]

      [8] LI Li(李莉), MA Yu(马禹), CAO Yan-Zhen(曹艳珍), et al. Acta Phys.-Chim. Sin.(Wuli Huaxue Xuebao), 2009,25(7): 1461-1466

    9. [9]

      [9] He Z Y, Li Y G, Zhang Q G, et al. Appl. Catal. B, 2010,93 (3/4): 376-382

    10. [10]

      [10] Xu L, Steinmiller E M P, Skrabalak S E. J. Phys. Chem. C, 2010,116(1):871-877

    11. [11]

      [11] Chen D, Zhang H, Hu S, et al. J. Phys. Chem. C, 2008,112 (1):117-122

    12. [12]

      [12] Lin D D, Hui W, Zhang R, et al. J. Chem. Mater., 2009,21 (15):3479-3484

    13. [13]

      [13] Lu W W, Gao S Y, Wang J J. J. Phys. Chem. C, 2008,112 (43):16792-16800

    14. [14]

      [14] Kuai L, Geng B Y, Chen X T, et al. Langmuir., 2010,26(24): 18723-18727

    15. [15]

      [15] Yang Z J, Lv L L, Dai Y L, et al. Appl. Surf. Sci., 2010,256 (9):2898-2902

    16. [16]

      [16] Yang Y Q, Du G H, Xin X, et al. Appl. Phys. A, 2011,104 (4):1229-1235

    17. [17]

      [17] LI Li(李莉), ZHUO Na(禚娜), GAO Yu(高宇), et al. Chem. J. Chinese Universities(Gaodeng XueXiao Huaxue Xuebao), 2012,33(6):1264-1270

    18. [18]

      [18] Zhang H, Wang G, Chen D, et al. Chem. Mater., 2008,20 (20):6543-6549

    19. [19]

      [19] Sasaoka E, Sada N, Manabe A, et al. Ind. Eng. Chem. Res., 1999,38(3):958-963

    20. [20]

      [20] Nolan N T, Seery M K, Pillai S C. Chem. Mater., 2011,23(6): 1496-1504

    21. [21]

      [21] Liu R L, Huang Y X, Xiao A H, et al. J. Alloys Compd., 2010,503(1):103-110

    22. [22]

      [22] Wang T, Jiang X, Mao C W. Langmuir, 2008,24(24):14042- 14047

    23. [23]

      [23] Sun T J, Qiu J S, Liang C H. J. Phys. Chem. C, 2008,112 (3):715-721

    24. [24]

      [24] Ou H H, Lo S L, Liao C H. J. Phys. Chem. C, 2011,115 (10):4000-4007

    25. [25]

      [25] Wu T S, Wang K X, Li G D, et al. ACS. Appl Mater&Inter., 2010,2(2):544-550

    26. [26]

      [26] Moulder J F, Stick W F, Sobol P E, et al. Handbook of X- ray Photoelectron Spectroscopy [M] . Eden Prairie: Perkin- Elmer. Corp, 1992:pp182183

    27. [27]

      [27] Ren W, Ai Z, Jia F, et al. Appl. Catal. B, 2007,69(3/4):138- 144

    28. [28]

      [28] Xin B F, Jing L Q, Ren Z Y, et al. J. Phys. Chem. B, 2005, 109(7):2805-2809

    29. [29]

      [29] Poyraz A S, Dag O. J. Phys. Chem. C, 2009,113(43):18596- 18607

    30. [30]

      [30] Sing K S W, Everett D H, Haul R A W. Pure. Appl. Chem., 1985,57(4):603-619

    31. [31]

      [31] ZOU Wen(邹文), HAO Wei-Chang(郝维昌), XIN Xin(信心), et al. Chinese J. Inorg. Chem. (Wuji Huaxue Xuebao), 2009, 25(11):1971-1976

    32. [32]

      [32] Wen Z H, Wang G, Lu W, et al. Cryst. Growth Des., 2007,7 (9):1722-1725

    33. [33]

      [33] Sudeep P K, Kamat P V. Chem. Mater., 2010,17(22):5404- 5410

    34. [34]

      [34] Gu C D, Cheng C C, Huang H Y, et al. Cryst. Growth Des., 2009,9(7):3278-3285

    35. [35]

      [35] Ldgar M, Jancar B, Sturm S, et al. Langmuir, 2010,26(14): 12215-12224

    36. [36]

      [36] Lei Y Z, Zhao G H, Liu M C, et al. J. Phys. Chem. C, 2009, 113(44):19067-19076

  • 加载中
    1. [1]

      Xia ZHANG , Yushi BAI , Xi CHANG , Han ZHANG , Haoyu ZHANG , Liman PENG , Shushu HUANG . Preparation and photocatalytic degradation performance of rhodamine B of BiOCl/polyaniline. Chinese Journal of Inorganic Chemistry, 2025, 41(5): 913-922. doi: 10.11862/CJIC.20240255

    2. [2]

      Yuanqing Wang , Yusong Pan , Hongwu Zhu , Yanlei Xiang , Rong Han , Run Huang , Chao Du , Chengling Pan . Enhanced Catalytic Activity of Bi2WO6 for Organic Pollutants Degradation under the Synergism between Advanced Oxidative Processes and Visible Light Irradiation. Acta Physico-Chimica Sinica, 2024, 40(4): 2304050-0. doi: 10.3866/PKU.WHXB202304050

    3. [3]

      Xinxin YU , Yongxing LIU , Xiaohong YI , Miao CHANG , Fei WANG , Peng WANG , Chongchen WANG . Photocatalytic peroxydisulfate activation for degrading organic pollutants over the zero-valent iron recovered from subway tunnels. Chinese Journal of Inorganic Chemistry, 2025, 41(5): 864-876. doi: 10.11862/CJIC.20240438

    4. [4]

      Kun WANG , Wenrui LIU , Peng JIANG , Yuhang SONG , Lihua CHEN , Zhao DENG . Hierarchical hollow structured BiOBr-Pt catalysts for photocatalytic CO2 reduction. Chinese Journal of Inorganic Chemistry, 2024, 40(7): 1270-1278. doi: 10.11862/CJIC.20240037

    5. [5]

      Jingyu Cai ,  Xiaoyu Miao ,  Yulai Zhao ,  Longqiang Xiao . Exploratory Teaching Experiment Design of FeOOH-RGO Aerogel for Photocatalytic Benzene to Phenol. University Chemistry, 2024, 39(4): 169-177. doi: 10.3866/PKU.DXHX202311028

    6. [6]

      Zhuo WANG , Junshan ZHANG , Shaoyan YANG , Lingyan ZHOU , Yedi LI , Yuanpei LAN . Preparation and photocatalytic performance of CeO2-reduced graphene oxide by thermal decomposition. Chinese Journal of Inorganic Chemistry, 2024, 40(9): 1708-1718. doi: 10.11862/CJIC.20240067

    7. [7]

      Xuejiao Wang , Suiying Dong , Kezhen Qi , Vadim Popkov , Xianglin Xiang . Photocatalytic CO2 Reduction by Modified g-C3N4. Acta Physico-Chimica Sinica, 2024, 40(12): 2408005-0. doi: 10.3866/PKU.WHXB202408005

    8. [8]

      Jianyin He , Liuyun Chen , Xinling Xie , Zuzeng Qin , Hongbing Ji , Tongming Su . Construction of ZnCoP/CdLa2S4 Schottky Heterojunctions for Enhancing Photocatalytic Hydrogen Evolution. Acta Physico-Chimica Sinica, 2024, 40(11): 2404030-0. doi: 10.3866/PKU.WHXB202404030

    9. [9]

      Ruolin CHENG , Haoran WANG , Jing REN , Yingying MA , Huagen LIANG . Efficient photocatalytic CO2 cycloaddition over W18O49/NH2-UiO-66 composite catalyst. Chinese Journal of Inorganic Chemistry, 2024, 40(3): 523-532. doi: 10.11862/CJIC.20230349

    10. [10]

      Yulian Hu ,  Xin Zhou ,  Xiaojun Han . A Virtual Simulation Experiment on the Design and Property Analysis of CO2 Reduction Photocatalyst. University Chemistry, 2025, 40(3): 30-35. doi: 10.12461/PKU.DXHX202403088

    11. [11]

      Ronghui LI . Photocatalysis performance of nitrogen-doped CeO2 thin films via ion beam-assisted deposition. Chinese Journal of Inorganic Chemistry, 2025, 41(6): 1123-1130. doi: 10.11862/CJIC.20240440

    12. [12]

      Tong WANG , Qinyue ZHONG , Qiong HUANG , Weimin GUO , Xinmei LIU . Mn-doped carbon quantum dots/Fe-doped ZnO flower-like microspheres heterojunction: Construction and photocatalytic performance. Chinese Journal of Inorganic Chemistry, 2025, 41(8): 1589-1600. doi: 10.11862/CJIC.20250011

    13. [13]

      Tong Zhou , Xue Liu , Liang Zhao , Mingtao Qiao , Wanying Lei . Efficient Photocatalytic H2O2 Production and Cr(Ⅵ) Reduction over a Hierarchical Ti3C2/In4SnS8 Schottky Junction. Acta Physico-Chimica Sinica, 2024, 40(10): 2309020-0. doi: 10.3866/PKU.WHXB202309020

    14. [14]

      Linfeng Xiao , Wanlu Ren , Shishi Shen , Mengshan Chen , Runhua Liao , Yingtang Zhou , Xibao Li . Enhancing Photocatalytic Hydrogen Evolution through Electronic Structure and Wettability Adjustment of ZnIn2S4/Bi2O3 S-Scheme Heterojunction. Acta Physico-Chimica Sinica, 2024, 40(8): 2308036-0. doi: 10.3866/PKU.WHXB202308036

    15. [15]

      Jiawei Hu , Kai Xia , Ao Yang , Zhihao Zhang , Wen Xiao , Chao Liu , Qinfang Zhang . Interfacial Engineering of Ultrathin 2D/2D NiPS3/C3N5 Heterojunctions for Boosting Photocatalytic H2 Evolution. Acta Physico-Chimica Sinica, 2024, 40(5): 2305043-0. doi: 10.3866/PKU.WHXB202305043

    16. [16]

      Guoqiang Chen , Zixuan Zheng , Wei Zhong , Guohong Wang , Xinhe Wu . Molten Intermediate Transportation-Oriented Synthesis of Amino-Rich g-C3N4 Nanosheets for Efficient Photocatalytic H2O2 Production. Acta Physico-Chimica Sinica, 2024, 40(11): 2406021-0. doi: 10.3866/PKU.WHXB202406021

    17. [17]

      Xin Zhou ,  Zhi Zhang ,  Yun Yang ,  Shuijin Yang . A Study on the Enhancement of Photocatalytic Performance in C/Bi/Bi2MoO6 Composites by Ferroelectric Polarization: A Recommended Comprehensive Chemical Experiment. University Chemistry, 2024, 39(4): 296-304. doi: 10.3866/PKU.DXHX202310008

    18. [18]

      Jingzhuo Tian , Chaohong Guan , Haobin Hu , Enzhou Liu , Dongyuan Yang . Waste plastics promoted photocatalytic H2 evolution over S-scheme NiCr2O4/twinned-Cd0.5Zn0.5S homo-heterojunction. Acta Physico-Chimica Sinica, 2025, 41(6): 100068-0. doi: 10.1016/j.actphy.2025.100068

    19. [19]

      Chenye An , Sikandaier Abiduweili , Xue Guo , Yukun Zhu , Hua Tang , Dongjiang Yang . Hierarchical S-scheme Heterojunction of Red Phosphorus Nanoparticles Embedded Flower-like CeO2 Triggering Efficient Photocatalytic Hydrogen Production. Acta Physico-Chimica Sinica, 2024, 40(11): 2405019-0. doi: 10.3866/PKU.WHXB202405019

    20. [20]

      Qin Hu , Liuyun Chen , Xinling Xie , Zuzeng Qin , Hongbing Ji , Tongming Su . Construction of Electron Bridge and Activation of MoS2 Inert Basal Planes by Ni Doping for Enhancing Photocatalytic Hydrogen Evolution. Acta Physico-Chimica Sinica, 2024, 40(11): 2406024-0. doi: 10.3866/PKU.WHXB202406024

Get Citation
PDF
XML
Metrics
  • PDF Downloads(452)
  • Abstract views(722)
  • HTML views(104)

通讯作者: 陈斌, bchen63@163.com
  • 1. 

    沈阳化工大学材料科学与工程学院 沈阳 110142

  1. 本站搜索
  2. 百度学术搜索
  3. 万方数据库搜索
  4. CNKI搜索
Address：Zhongguancun North First Street 2,100190 Beijing, PR China Tel: +86-010-82449177-888
Powered By info@rhhz.net

/

DownLoad:  Full-Size Img  PowerPoint
Return