Citation: LONG Qin, ZHOU Dali, ZHANG Xiang, WEI Dong-Juan, LIU Shu-Jing, CHEN Dong-Lin. Preparation of a Silane Coupling Agent and Surface Modification of Apatite-Wollastonite Bioactive Glass-Ceramic[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(5): 948-952. doi: 10.3969/j.issn.1001-4861.2013.00.147 shu

Preparation of a Silane Coupling Agent and Surface Modification of Apatite-Wollastonite Bioactive Glass-Ceramic

1.
College of Materials Science and Engineering, Sichuan University, Chengdu 610064, China

Corresponding author: ZHOU Dali,
Received Date: 19 October 2012
Available Online: 7 January 2013
Fund Project: 四川大学2011年青年基金(No.2082604154120)资助项目。 (No.2082604154120)

In this work, a kind of silane coupling agent was prepared by condensation reaction of the glutamic acid and silane coupling agent (KH-792). The Glutamic acid was attached to the surface of Apatite-wollastonite bioactive glass-ceramic (A-W GC) by the bifunctional cross-linking agent. To evaluate in vitro cytocompatibility, the surface modified material was co-cultured with the 5th generation human osteosarcoma cell MG63. Fourier Transform infrared spectroscopy (FTIR), Scanning Electron Microscope (SEM), and X-ray Photoelectron Spectroscopy (XPS) were used to character the structure and performance of the synthetic coupling agent and the surface modified A-W GC, respectively. The results show that the Glutamic acid and KH-792 were connected by amide groups, and A-W GC is effectively modified by the synthetic coupling agent. The MG63 cell experiments show that cells adhered to the surface of the material, and the cell proliferation on the surface of the material was promoted. It is an effective method to improve the cell compatibility of A-W GC by surface modification.
- silane coupling agent;glutamic acid;apatite-wollastonite bioactive glass-ceramic;surface modification
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沈阳化工大学材料科学与工程学院沈阳 110142