Citation: LUO Fei, ZHOU De-Feng, YANG Guo-Cheng, LIU Jian-Wei, LI Zhao-Hui, MENG Jian. Electrospinning Preparation and Visible-Light Photocatalytic Activity of V2O5 Micro-Nanorod[J]. Chinese Journal of Inorganic Chemistry, ;2013, 29(3): 500-506. doi: 10.3969/j.issn.1001-4861.2013.00.104
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V2O5 micro-nanorods were fabricated via calcining the as-synthesized precursors prepared by electrospinning technique route using NH4VO3 and PVP as regent. The physicochemical properties of the catalysts were characterized by Thermogravimetric and Differential thermal analysis (TG-DTA), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (FE-SEM), X-ray photoelectron spectroscopy (XPS) and UV-Vis diffuse reflectance spectra(UV-Vis). The photocatalytic activity of V2O5 micro-nanorod toward the decomposition of Methylene Blue (MB) was investigated. The results indicated that calcination temperature had a great influence on the morphologies and crystalline phases of the micro-nanorod. 550 ℃ micro-nanorod exhibited the highest activity for degrading MB under Visible light, and the photocatalytic mechanism of V2O5 micro-nanorod was also presented.
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