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Citation: LV Renjiang, ZHANG Fuxiang, LI Yingjie, WANG Lina, WU Jing, DING Li. Solvothermal Synthesis of Mesoporous Tungsten Oxide Materials with Special Morphology and Their Adsorptive Properties[J]. Chinese Journal of Applied Chemistry, ;2013, 30(11): 1338-1342. doi: 10.3724/SP.J.1095.2013.20515 shu

Solvothermal Synthesis of Mesoporous Tungsten Oxide Materials with Special Morphology and Their Adsorptive Properties

Chemistry and Chemical Engineering Institute of Qiqihar University, Qiqihar 161006, China

Received Date: 8 November 2012
Revised Date: 1 April 2013

With the sodium tungstate as tungsten source,the mixture of water and alcohol solution as solvent,and triblock copolymer of ethylene oxide with propylene oxide (P123) as structure directing agent and porogen,mesoporous WO₃ of special morphology was synthesized by precursor route and solvothermal method,and meanwhile the influence of different reaction time and temperature were also discussed. These samples were characterized and analyzed by the X-ray diffraction (XRD),scanning electron microscope (SEM),transmission electric microscope (TEM),N₂ adsorption-desorption,UV-visible spectroscopy,and the thermo gravimetric (TG). The results show that the as-prepared WO₃ materials possess mesoporous structure and large specific surface area,moreover,the increasing of the solvothermal time and reaction temperature are beneficial to the size enlargement and also the morphology variance of the WO₃ particles. Absorption test of the synthesized mesoporous WO₃ materials for rhodamine B dye in aqueous solution was also performed,and a good adsorption performance with a removal efficiency of 93.13% was achieved.
- solvothermal method,
- special morphology,
- mesoporous,
- tungsten oxide,
- adsorption performance
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