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Citation: FAN Xuemei, WANG Shumin, LI Qian, WANG Xiangting, WANG Xiansheng, CHEN Fengying. Determination of 5-Sulfosalicylic Acid in the Waste Water by NBS-Dichlorofluoresce in Chemiluminescence System[J]. Chinese Journal of Applied Chemistry, ;2013, 30(4): 469-473. doi: 10.3724/SP.J.1095.2013.20246 shu

Determination of 5-Sulfosalicylic Acid in the Waste Water by NBS-Dichlorofluoresce in Chemiluminescence System

Department of Chemistry and Chemical Engineering, Shangluo College, Shanxi Shangluo 726000, China

Received Date: 5 June 2012
Revised Date: 5 August 2012

A new flow-injection chemiluminescence method for the determination of 5-sulfosalicylic acid was proposed.Various factors affected the chemiluminescence signal were investigated and the possible mechanism was also studied.Under the optimum conditions,the linear range for the determination of 5-sulfosalicylic acid was 5.0 × 10^-8~2.0 × 10^-5 mol/L with a detection limit(S/N=3) of 1.0 × 10^-8 mol/L. The relative standard deviation was 2.7% for 5.0 × 10^-6 mol/L 5-sulfosalicylic acid solution in nine repeated measurements. The method was successfully applied to the determination of 5-sulfosalicylic acid in the waste water of doxycycline.
- flow-injection,
- chemiluminescence,
- dichlorofluorescein,
- sulfosalicylic acid
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