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Citation: XU Ling, KAN Qiubin. Synthesis and Characterization of the Hierarchical Porous Aluminosilicate Material[J]. Chinese Journal of Applied Chemistry, ;2011, 28(4): 478-482. doi: 10.3724/SP.J.1095.2011.00505 shu

Synthesis and Characterization of the Hierarchical Porous Aluminosilicate Material

XU Ling ^a ,
KAN Qiubin ^b,,

1.
a College of Chemistry and Chemical Engineering, Inner Mongolia University for Nationalities, Tongliao;
2.
b College of Chemistry, Jilin University, Changchun 130021

Corresponding author: KAN Qiubin,
Received Date: 29 August 2010
Available Online: 25 December 2010
Fund Project: 国家自然科学基金(20673046)资助项目 (20673046)内蒙古自治区高等学校科研项目(NJzy08084) (NJzy08084)

The hierarchical porous aluminosilicate material was obtained by hydrothermal treatment and calcination of the precursor prepared using polystyrene spheres coated with polyelectrolyte as the template.The hierarchical porous materials were characterized by XRD,FT-IR,N₂ adsorption-desorption,SEM and TEM.In addition,the influence of crystallized time on the porous structures was studied.The results show that the material contained meso-macropore with hydrothermal treatment of less than 22 h.However,the sample exhibits micro-meso-macroporous structures when the crystallized time was more than 22 h.In particular,the XRD and SEM results exhibit that the wall of macro-pore was composed of nano-ZSM-5 zeolite when the sample was crystallized for 36 h.
- hierarchical porous,
- aluminosilicate material,
- layer-by-layer self-assembly
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