Citation: WANG Wei, ZHENG Fei, GE Yan, QIAO Mengdan, YUE Hao, LIU Shuying. Analysis of Volatile Components in Processed Ginseng by GC-MS/MS[J]. Chinese Journal of Applied Chemistry, ;2017, 34(8): 965-970. doi: 10.11944/j.issn.1000-0518.2017.08.160481 shu

Analysis of Volatile Components in Processed Ginseng by GC-MS/MS

  • Corresponding author: YUE Hao, yuehao@sohu.com
  • Received Date: 29 November 2016
    Revised Date: 20 December 2016
    Accepted Date: 20 January 2017

    Fund Project: the National Natural Science Foundation of China No.3140040275Supported by the National Natural Science Foundation of China(No.3140040275)

Figures(2)

  • The research of chemical changes in ginseng processing has been focusing on saponins and sugars. In this paper, volatile components in ginseng were studied for the first time, which provide a substance basis for different processed ginseng. The volatile components and their derivative paths of fresh ginseng, sun-dry ginseng and red ginseng were studied by gas chromatography-mass spectrometry(GC-MS/MS). The volatile components were detected and analyzed using TG-5SILMS nonpolar GC column, with He as the carrier gas through the NIST MS Spectral Database. Thirty, thirty-three and thirty-four species of volatile compounds in fresh ginseng, sun-dry ginseng and red ginseng were detected, respectively. The content of (-)-spartak alcohol in sun-dry ginseng is 31.98 times higher than that in the fresh ginseng, while the levels of eight volatile components such as octanal in sun-dry ginseng is three times higher than those in the fresh ginseng. The contents of ten volatile components such as cyclodecanone in red ginseng are 3 times higher than those in the fresh ginseng. Four volatile compounds in sun-dry ginseng and in red ginseng are not detected in fresh ginseng.
  • 加载中
    1. [1]

      DAI Yulin, YUE Hao, SUN Changjiang. Determination of Ginsenosides in Processed Ginseng by Rapid Resolution Liquid Chromatography Coupled with Quadrupole-Time-of-Flight Tandem Mass Spectrometry[J]. Chinese J Anal Chem, 2015,43(8):1181-1186. doi: 10.11895/j.issn.0253-3820.150204

    2. [2]

      XU Jing, JIA Li, ZHAO Yuqing. Constituents of Ginseng and Quality Evaluation of Ginseng Products[J]. Drug Eval Res, 2011,34(3):199-202.  

    3. [3]

      LI Jing, DAI Yulin, ZHENG Fei. Oral Absorption and in vivo Biotransformation of Ginsenosides[J]. Chinese J Biol, 2014,27(12):1633-1636.  

    4. [4]

      HAN Dong, ZHANG Tiejun, TANG Cheng. Research Progress on Pharmacokinetics of Panax Ginseng Saponins[J]. Chinese Tradit Herb Drugs, 2009,40(2):附1-附3.  

    5. [5]

      REN Ming, HAO Xiaoshi, YE Lingyan. Extraction and Isolation of Polysaccharide from Ginseng and Its Anti-tumor Activity in vitro[J]. J Jilin Univ(Med Ed), 2014,40(4):812-815.  

    6. [6]

      ZHAO Hua, WEI Jianhua, XU Tao. Analysis of Volatile Oil Components of Panax Ginseng by GC-MS[J]. Ginseng Res, 2014(3):45-48.  

    7. [7]

      YANG Ling, DAN Dan, ZHU Rui. β-Elemene Inhibits Expression of ANGⅡ and RhoA/ROCK Signaling in Hepatic Stellate Cells[J]. J Chinese Mater Med, 2009,34(4):458-462.  

    8. [8]

      XU Liying, ZHANG Xingzhong, DU Huilian. Synthesis and Antitumor Activity of β-Elemene Derivatives Bearing Amino Acid Moiety[J]. Chinese J Med Chem, 2013,23(3):169-175.  

    9. [9]

      Kobaisy M, Abramowski Z, Lermer L. Antimycobacterial Polyynes of Devil's Club(Oplopanax horridus), a North American Native Medicinal Plant[J]. J Nat Prod, 1997,60:1210-1213. doi: 10.1021/np970182j

    10. [10]

      Sohn J, Lee C H, Chung D J. Effect of Petroleum Ether Extract of Panax Ginseng Roots on Proliferation and Cell Cycle Progression of Human Renal Cell Carcinoma Cells[J]. Exp Mol Med, 1998,30(1):47-51. doi: 10.1038/emm.1998.7

    11. [11]

      DUAN Xianchun, XIA Lunzhu, WANG Yongzhong. Protective Effects of Panaxynol on Nerve Cells under Oxygen and Glucose Deprivation[J]. Chinese J Exp Tradit Med Formulae, 2011,17(16):180-183. doi: 10.3969/j.issn.1005-9903.2011.16.052

    12. [12]

      Xing J, Sun H M, Li Z Y. Comparison of Volatile Components Between Raw and Vinegar Baked Radix Bupleuri by GC-MS Based Metabolic Fingerprinting Approach[J]. Evid-Based Compl Alter Med, 2015:1-7.

    13. [13]

      Aranda-Rodriguez R, Cabecinha A, Harvie J. A Method for Quantification of Volatile Organic Compounds in Blood by SPME-GC-MS/MS with Broader Application; From Non-Occupational Exposure Population to Exposure Studies[J]. J Chromatogr B Anal Technol Biomed Life Sci, 2015(992):76-85.

    14. [14]

      Ma X Y, Zhang L H, Shao H B. Jerusalem Artichoke(Helianthus tuberosus L.), a Medicinal Salt-Resistant Plant has High Adaptability and Multiple-Use Values[J]. J Med Plants Res, 2011,5(8):1275-1282.

    15. [15]

      Zead H, Khaldun M Al A, Yuliya T. Analysis of Essential Oil in Jerusalem Artichoke(Helianthus tuberosus L.) Leaves and Tubers by Gas Chromatography-Mass Spectrometry[J]. Adv Pharm Bull, 2014,4(Suppl 2):521-526.

    16. [16]

      MAHEMUTI Maimaitiming, MILIBAN Nuojia, MAERHABA Wusiman. Analysis of Volatile Oils and Fatty Acids in Tamarix Chinensis Fruit[J]. Chinese J Appl Chem, 2015,32(2):239-244. doi: 10.11944/j.issn.1000-0518.2015.02.140136 

    17. [17]

      LI Xiaoli, LIU Baofeng, XIE Wenbing. The Contrastive Analysis of Puffballs Produced from Inner Mongolia and Jilin[J]. Chinese J Appl Chem, 2012,29(4):477-482.  

    18. [18]

      LIN Zhaozhan, ZHU Chenchen, ZHANG Cuixian. Studies on Chemical Constituents and Antioxidant Activity of Essential Oil from Leaves of Eucommia[J]. J Trop Subtrop Botany, 2009,17(4):401-405.  

    19. [19]

      Shinji T, Denan J, Kazuyoshi K. Effects of a Lipoxygenase Inhibitor, Panaxynol, on Vascular Contraction Induced by Angiotensin Ⅱ[J]. Jpn J Pharm, 1999,80(1):89-92. doi: 10.1254/jjp.80.89

    20. [20]

      Fujimoto Y, Sakuma S, Komatsu S. Inhibition of 15-Hydroxyprostahlandin Dehydrogenase Activity in Rabbit Gastricantral Mucosa by Panaxynol Isolated from Oriental Medicines[J]. J Pharm Pharmacol, 1998,50(9):1075-1078. doi: 10.1111/jphp.1998.50.issue-9

    21. [21]

      ZOU Kun, ZHU Shu, CAI Shaoqing. HPLC/UV Analysjs of Lipid Extract from Panax Ginseng Roots with Neural Outgrowth Activity[J]. J China Three Gorges Univ(Nat Sci), 2002,24(4):155-160.  

    22. [22]

      SONG Yang. Optimization of Extraction Technology and Chemical Constituents of Volatile Oil from Root of the Root[J]. Shanxi Med J, 2014,43(5):487-489.  

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