Citation: Yue ZHUO, Zhihao LIU, Yixuan LIU, Caifu QIU, Haiquan YAO, Xin QIU, Yan PENG, Zhaobo HU. A zero-dimensional manganese(Ⅱ)-based hybrid with high-temperature phase transitions and synergistic dielectric, magnetic and luminescent switching responses[J]. Chinese Journal of Inorganic Chemistry, ;2026, 42(11): 2362-2370. doi: 10.11862/CJIC.20260178 shu

A zero-dimensional manganese(Ⅱ)-based hybrid with high-temperature phase transitions and synergistic dielectric, magnetic and luminescent switching responses

Yue ZHUO ¹ ,
Zhihao LIU ² ,
Yixuan LIU ² ,
Caifu QIU ² ,
Haiquan YAO ² ,
Xin QIU ^1,, ,
Yan PENG ^2,, ,
Zhaobo HU ^2,,

1.
School of Information Engineering, Jiangxi University of Science and Technology, Ganzhou, Jiangxi 341000, China
2.
School of Chemistry and Chemical Engineering, Jiangxi University of Science and Technology, Ganzhou, Jiangxi 341000, China

Corresponding author: Xin QIU, qiuxinswu@163.com Yan PENG, py16882020@163.com Zhaobo HU, huzhaobo@smail.nju.edu.cn
Received Date: 3 June 2026
Revised Date: 3 September 2026

Figures(7)

A novel manganese-based hybrid material (TMBE)₂[MnBr₄] (1) was successfully synthesized via the slow evaporation method, using (2-bromoethyl)trimethylammonium bromide ((TMBE)Br) and MnBr₂·4H₂O. Single-crystal structural analysis reveals that 1 crystallizes in the Pca2₁ space group, with Mn²⁺ coordinating with Br^- to form isolated tetrahedra, while the organic cation separates the inorganic anions, resulting in a zero-dimensional crystal structure. Differential scanning calorimetry measurements demonstrate that compound 1 undergoes a reversible first-order phase transition with a maximum phase transition temperature of 413 K. Dielectric, variable-temperature fluorescence, and magnetic measurements showed that compound 1 exhibited synchronous switching behavior of dielectric constant, luminous intensity, and magnetization near 344 K. These results indicate that halogen substitution on organic cations is an effective strategy for constructing high-temperature phase-transition materials that integrate dielectric, optical, and magnetic synergistic responses triggered by structural phase transitions.
- phase transition,
- dielectric,
- luminescence,
- magnetism,
- synergistic response
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