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Citation: Qing ZHANG, Kexin ZHOU, Yanjun GUO, Guangjun CHEN, Bai HE, Bo YU, Songshan JIANG, Guoyuan YUAN, Huidong QIU. Preparation, functional modification, and applications of Fe3O4 nanoparticles[J]. Chinese Journal of Inorganic Chemistry, ;2026, 42(7): 1383-1411. doi: 10.11862/CJIC.20250344 shu

Preparation, functional modification, and applications of Fe3O4 nanoparticles

  • 1.

    College of Chemistry and Chemical Engineering, Chongqing University of Science and Technology, Chongqing 401331, China

  • 2.

    Northwest Sichuan Gas District, Petro China Southwest Oil& Gasfield Company, Mianyang, Sichuan 621700, China

  • Corresponding author: Bai HE, hbai2004@126.com
  • Received Date: 30 November 2025
    Revised Date: 11 May 2026

Figures(12)

  • Magnetic nanoparticles (MNPs), a class of nanoscale magnetic materials, possess excellent mechanical properties, high surface activity, and remarkable selectivity, which have established them as a prominent research focus in the field of advanced materials. Among various types of MNPs, Fe3O4 nanoparticles (Fe3O4 NPs) exhibit distinct characteristics, including superparamagnetism, high coercivity, and a low Curie temperature. Thus, Fe3O4 NPs have been widely utilized as adsorbents, catalysts, and drug carriers in areas including environmental remediation, chemical synthesis, and biomedical therapies, exhibiting great potential for further development. The common preparation methods for Fe3O4 NPs, such as co-precipitation, thermal decomposition, sol-gel synthesis, and ball milling, have been systematically reviewed, and their respective advantages and limitations have been critically evaluated. For instance, the co-precipitation method enables the synthesis of Fe3O4 NPs with tunable particle sizes and morphologies by adjusting reaction parameters. However, the as-synthesized nanoparticles are highly susceptible to agglomeration and oxidation. The solvothermal route can yield Fe3O4 NPs with relatively small particle dimensions and uniform morphology, yet the crystallinity of the products may be limited, and the process tends to be costly. Although the sol-gel method features procedural simplicity, fewer synthetic steps, and high crystallinity of the resultant nanoparticles, it is plagued by low efficiency, high cost, and great challenges in scaling up for industrial production. Ball milling, while operationally simple, safe, and capable of high throughput, provides inadequate control over particle size and properties, necessitating strict control of processing parameters. Moreover, based on the integration strategies for combining functional materials with Fe3O4 NPs, surface modification and functionalization techniques are classified into several categories, including coating, loading, doping, and grafting, and the progress in each of these functionalization approaches has been summarized and discussed. Furthermore, the applications and emerging trends of Fe3O4 NPs and their composites in wastewater treatment, catalytic processes, biomedicine, and related fields have been comprehensively reviewed. Finally, future perspectives are put forward regarding the scalable production of Fe3O4 NPs via integrated methodologies, the development of more efficient and versatile functionalization protocols, and the exploration of their performance in complex operational environments.
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