Citation: Yang WANG, Lulu ZHANG, Hanjiang HE, Xia ZHANG, Xiaohong SUN, Fan WANG, Shuli WANG. In situ construction of ammonium phosphomolybdate@ZIF-8 composite for Rb⁺ and Cs⁺ adsorption performance[J]. Chinese Journal of Inorganic Chemistry, ;2026, 42(4): 826-842. doi: 10.11862/CJIC.20250332 shu

In situ construction of ammonium phosphomolybdate@ZIF-8 composite for Rb⁺ and Cs⁺ adsorption performance

Yang WANG ^{1, 2,,} ,
Lulu ZHANG ^{3, 4} ,
Hanjiang HE ¹ ,
Xia ZHANG ¹ ,
Xiaohong SUN ¹ ,
Fan WANG ^1,, ,
Shuli WANG ^1,,

1.
Geology Institute of China, Chemical Geology and Mine Bureau, Beijing 100101, China
2.
College of Science, Hebei Agricultural University, Baoding, Hebei 071001, China
3.
BGRIMM MTC Technology Co., Ltd., Beijing 102628, China
4.
National Center for Quality Inspection and Testing of Heavy Non⁃Ferrous Metals, Beijing 102628, China

Corresponding author: Yang WANG, wjxzllwy@163.com Fan WANG, severalpoint@126.com Shuli WANG, wangshuli77@126.com
Received Date: 3 November 2025
Revised Date: 12 December 2025

Figures(9)

A metal-organic framework/inorganic composite (ZIF-8@AMP) was synthesized by the in situ introduction of the active component ammonium phosphomolybdate (AMP) during the ambient solution-phase synthesis of the metal-organic framework (ZIF-8). The structure and properties of the composite were characterized using scanning electron microscopy (SEM), X-ray powder diffraction (XRD), X-ray photoelectron spectroscopy (XPS), thermogravimetric analysis (TGA), and Fourier transform infrared spectroscopy (FTIR). Its adsorption performance for Rb⁺ and Cs⁺ in water was investigated. Results indicate that ZIF-8@AMP exhibited adsorption efficiencies of 93.5% and 95.6% for Rb⁺ and Cs⁺ within 30 min, with maximum adsorption capacities of 92.7 and 104.5 mg·g^-1, respectively. After five adsorption-desorption cycles, it maintained high adsorption capacity and achieved over 84.9% adsorption efficiency for Rb⁺ and Cs⁺ in actual brine samples. The adsorption of ZIF-8@AMP for Rb⁺ and Cs⁺ follows pseudo-second-order kinetics and the Langmuir adsorption isotherm, indicating an endothermic, entropy-increasing, and spontaneous process. The adsorption mechanism involves electrostatic attraction and ion exchange between ZIF-8@AMP and Rb⁺ and Cs⁺.
- ammonium phosphomolybdate,
- ZIF-8,
- rubidium,
- cesium,
- adsorption
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In situ construction of ammonium phosphomolybdate@ZIF-8 composite for Rb+ and Cs+ adsorption performance

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In situ construction of ammonium phosphomolybdate@ZIF-8 composite for Rb⁺ and Cs⁺ adsorption performance