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Citation: Xian XIA, Qin SHI, Wanyi SU, Qingjun XUE, Honghui PAN, Xixiang LIU, Chuanqi ZHAO. In-situ synthesis of Bi2O3@BiVO4 composite via solvothermal method and its adsorption performance for rhodamine B in water[J]. Chinese Journal of Inorganic Chemistry, ;2026, 42(5): 1096-1112. doi: 10.11862/CJIC.20250311 shu

In-situ synthesis of Bi2O3@BiVO4 composite via solvothermal method and its adsorption performance for rhodamine B in water

  • 1.

    Guangxi Key Laboratory of Advanced Structural Materials and Carbon Neutralization, Guangxi Engineering Research Center for Advanced Materials and Intelligent Manufacturing, School of Materials and Environment, Guangxi Minzu University, Nanning 530105, China

  • 2.

    Guangxi Xinjing Technology Co., Ltd., Nanning 530001, China

Figures(8)

  • Bi2O3@BiVO4 composites were synthesized using the solvothermal method with ethylene glycol as the solvent. Bi2O3 was grown on the surface of BiVO4 by regulating the reaction temperature. The adsorption performance of the composite for rhodamine B (RhB) was investigated. The results indicate that the reaction temperature significantly impacts the morphology and adsorption performance of Bi2O3@BiVO4. The Bi2O3@BiVO4 composite prepared at 180 ℃ (180-BO@BVO) consisted of nanoparticles with an average size of 7 nm, featuring a higher concentration of oxygen vacancies on the surface, but with a lower specific surface area (only 1.2 m2·g-1). 180-BO@BVO, with oxygen species adsorbed at surface oxygen vacancies carrying a negative charge, achieved an impressive RhB removal efficiency of up to 83.0% through electrostatic interaction with RhB. The adsorption process follows the Langmuir isotherm and the pseudo-second-order kinetic model, suggesting that it is predominantly governed by chemical adsorption. After five cycles of adsorption experiments, the removal efficiency of RhB by composites remained basically unchanged (more than 80%), demonstrating excellent regeneration performance.
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