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Citation: Huiying ZHANG, Ping LI, Weixia DONG, Zhiwen HU, Qifu BAO, Qizheng DONG, Mingmin BAI, Wenqi LI. Photocatalytic performance of spheroidal nano Bi4Ti3O12 prepared by surfactant-assisted hydrothermal reaction[J]. Chinese Journal of Inorganic Chemistry, ;2026, 42(3): 551-561. doi: 10.11862/CJIC.20250269 shu

Photocatalytic performance of spheroidal nano Bi4Ti3O12 prepared by surfactant-assisted hydrothermal reaction

  • School of Materials Science and Engineering, Jingdezhen Ceramic University, Jingdezhen, Jiangxi 333403, China

  • Corresponding author: Weixia DONG, weixia_dong@sina.com
  • Received Date: 23 August 2025
    Revised Date: 11 December 2025

Figures(10)

  • The spherical Bi4Ti3O12 photocatalyst formed by self-assembly of nanosheets was successfully prepared via the hydrothermal method using tetrabutyl titanate (TBOT) and bismuth nitrate pentahydrate (Bi(NO3)3·5H2O) as precursors, assisted by two surfactants, sodium dodecyl sulfate (SDS) or sodium oleate. The structure and properties of the as-prepared materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), ultraviolet-visible absorption spectroscopy (UV-Vis), Fourier transform infrared spectroscopy (FTIR), and electrochemical impedance spectroscopy (EIS). The results indicated that the sample modified with surface surfactants reduced the band gap from 2.72 to 2.46 eV, thereby significantly enhancing light absorption. The photocatalytic performance of the catalysts was evaluated under UV light irradiation for the degradation of methylene blue (MB), rhodamine B (RhB), and methyl orange (MO). The Bi4Ti3O12 (BTO-1) prepared with SDS assistance exhibited the highest degradation rate of 98.9% for MB, while the Bi4Ti3O12 (BTO-2) prepared with sodium oleate assistance achieved the degradation rate of 98.5% for RhB, and kept the degradation rate of over 96% after five cyclic runs. Mechanism studies revealed that surface chemical modification effectively regulated the surface charge and hydrophobicity of the materials, leading to enhanced dye adsorption capacity. A synergistic mechanism of "surface modification-adsorption-photocatalysis" was therefore proposed.
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