Citation: Chenyang WANG, Yiyan BAI, Wei ZHANG, Zhaorong LIU, Yuchun WANG. Performance of photo-assisted copper oxide catalyzed hydrolysis of ammonia borane to produce hydrogen[J]. Chinese Journal of Inorganic Chemistry, ;2026, 42(1): 97-110. doi: 10.11862/CJIC.20250116 shu

Performance of photo-assisted copper oxide catalyzed hydrolysis of ammonia borane to produce hydrogen

Department of Applied Chemistry, Yuncheng University, Yuncheng, Shanxi 044000, China

Corresponding author: Chenyang WANG, wchy@ycu.edu.cn Yuchun WANG, 643709083@qq.com
Received Date: 3 April 2025
Revised Date: 2 December 2025

Figures(12)

A series of Cu₂O/CuO composite structures with adjustable valence states was successfully prepared by calcining nano-Cu₂O prepared by the liquid phase reduction method. The composite conventional catalytic performances under dark conditions and photo-assisted catalytic performances for hydrogen production by hydrolysis of ammonia borane were tested, respectively. The catalysts were systematically characterized by X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy, transmission electron microscopy, X-ray photoelectron spectroscopy, and a UV-visible spectrophotometer. The results show that the Cu₂O/CuO composite formed a raspberry-like nano-hollow sphere, in which the CuO content increases with increasing calcination time, and the absorption and utilization of visible light were enhanced compared to single-phase Cu₂O. Under visible light-assisted conditions, the rate of hydrogen production by catalytic hydrolysis of the composite structure could reach up to 150.09 mL·g^-1·min^-1, and the activation energy required for the reaction was only 37.1 kJ·mol^-1, which was significantly better than that under dark conditions. The Cu₂O/CuO catalyst underwent surface reconstruction to form Cu/Cu₂O/CuO during the catalytic hydrolysis of ammonia borane. The composite structure of metal and oxide provides a more efficient active hydrogen production process under visible light, thereby enhancing the catalytic activity.
- ammonia borane,
- hydrogen production by hydrolysis,
- catalyst,
- copper oxide,
- photo-assisted
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