Citation: Haifeng ZHENG, Xingzhe GUO, Yunwei WEI, Xinfang WANG, Huimin QI, Yuting YAN, Jie ZHANG, Bingwen LI. Post-synthetic modification strategy to construct Co-MOF composites for boosting oxygen evolution reaction activity[J]. Chinese Journal of Inorganic Chemistry, ;2026, 42(1): 193-202. doi: 10.11862/CJIC.20250029 shu

Post-synthetic modification strategy to construct Co-MOF composites for boosting oxygen evolution reaction activity

Haifeng ZHENG ^{1, #} ,
Xingzhe GUO ^{2, #} ,
Yunwei WEI ² ,
Xinfang WANG ^2,, ,
Huimin QI ² ,
Yuting YAN ² ,
Jie ZHANG ^3,, ,
Bingwen LI ^2,,

1.
Department of Physics and Electronic Information Engineering, Lyuliang University, Lüliang, Shanxi 033000, China
2.
College of Chemistry and Chemical Engineering, Dezhou University, Dezhou, Shandong 253023, China
3.
Department of Chemistry and Chemical Engineering, Taiyuan Institute of Technology, Taiyuan 030008, China

Corresponding author: Xinfang WANG, dzwxf@126.com Jie ZHANG, zhangjie@tit.edu.cn Bingwen LI, libingwen0609@163.com
Received Date: 24 January 2025
Revised Date: 1 December 2025

Figures(6)

The poor electrical conductivity of metal-organic frameworks (MOFs) limits their electrocatalytic performance in the oxygen evolution reaction (OER). In this study, a Py@Co-MOF composite material based on pyrene (Py) molecules and {[Co₂(BINDI)(DMA)₂]·DMA}_n (Co-MOF, H₄BINDI=N,N′-bis(5-isophthalic acid)naphthalenediimide, DMA=N,N-dimethylacetamide) was synthesized via a one-pot method, leveraging π-π interactions between pyrene and Co-MOF to modulate electrical conductivity. Results demonstrate that the Py@Co-MOF catalyst exhibited significantly enhanced OER performance compared to pure Co-MOF or pyrene-based electrodes, achieving an overpotential of 246 mV at a current density of 10 mA·cm^-2 along with excellent stability. Density functional theory (DFT) calculations reveal that the formation of O^* in the second step is the rate-determining step (RDS) during the OER process on Co-MOF, with an energy barrier of 0.85 eV due to the weak adsorption affinity of the OH^* intermediate for Co sites.
- pyrene,
- metal-organic frameworks,
- composite catalyst,
- oxygen evolution reaction,
- density functional theory
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