Citation: Zenkin Kubra, Dalmaz Aslihan, Ozdincer Mesut, Durmus Sefa. Anion effect on magnetic and structural properties of green synthesized NiO nanoparticles via Ni-salt precursors in Salvia officinalis extract[J]. Chinese Journal of Inorganic Chemistry, ;2024, 40(2): 451-462. doi: 10.11862/CJIC.20230090 shu

Anion effect on magnetic and structural properties of green synthesized NiO nanoparticles via Ni-salt precursors in Salvia officinalis extract

1.
Department of Chemistry, Graduate Education Institute, Duzce University, Duzce 81620, Türkiye
2.
Department of Natural and Herbal Products/Cosmetic Products, Graduate Education Institute, Duzce University, Duzce 81620, Türkiye
3.
Department of Composite-Materials, Graduate Education Institute, Duzce University, Duzce 81620, Türkiye
4.
Department of Chemistry, Faculty of Art and Science, Duzce University, Duzce 81620, Türkiye

Corresponding author: Zenkin Kubra, kubrazenkin@gmail.com
Received Date: 21 March 2023
Revised Date: 3 November 2023

Figures(9)

Using a green synthesis method, Salvia officinalis extract was used as a reducing and capping agent to synthesize nickel oxide nanoparticles (NiO NPs). In addition, NiO NPs were synthesized using various precursors, and their morphologies were analyzed using scanning electron microscopy. The structures of NiO NPs were characterized using Fourier-transform infrared spectroscopy, and powder X-ray diffraction (PXRD). Their magnetic properties were measured using a vibrating sample magnetometer. PXRD studies showed that all synthesized NiO NPs exhibited a face-centered cubic phase with high crystallinity, and NiO formations with a high-purity phase were confirmed. As a result of magnetization studies, NiO NPs synthesized from three nickel salt precursors (acetate, chloride, and sulfate) exhibit superparamagnetic, soft ferromagnetic, and paramagnetic behaviors, respectively.
- green synthesis,
- NiO nanoparticles,
- Salvia officinalis,
- anion effect,
- magnetic behavior
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