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Citation: Hua YANG, Yu-Pei FU, Dan QIAO, Lu-Lu DONG, Xiao-Li CHEN, Hua-Li CUI, Ji-Jiang WANG. Synthesis, crystal structure, magnetic properties, and photocatalytic activity of NiⅡ2ZnⅡ2 cluster complex based on 2-pyridinealdoxime ligand[J]. Chinese Journal of Inorganic Chemistry, ;2023, 39(11): 2219-2230. doi: 10.11862/CJIC.2023.186 shu

Synthesis, crystal structure, magnetic properties, and photocatalytic activity of NiⅡ2ZnⅡ2 cluster complex based on 2-pyridinealdoxime ligand

  • Shaanxi Key Laboratory of Chemical Reaction Engineering, Laboratory of New Energy and New Function Materials, School of Chemistry and Chemical Engineering, Yan'an University, Yan'an, Shaanxi 716000, China

  • Corresponding author: Hua YANG, yanghua_08@163.com
  • Received Date: 21 March 2023
    Revised Date: 1 October 2023

Figures(13)

  • Under solvothermal conditions, the reaction of 2-pyridinealdoxime (HL) with NiCl2·6H2O and Zn(OAc)2· 2H2O has led to a Ni2ⅡZn2Ⅱ cluster complex with composition[Ni2Zn2(L)4Cl2(CH3O)2] (1). This complex was characterized by elemental analysis, IR spectroscopy, single-crystal X-ray diffraction, etc. The results show that 1 belongs to the orthorhombic system with the Pna21 space group. The structure of 1 contains two NiⅡ ions, two ZnⅡ ions, two Cl- ions, four L- ligands, and two CH3O- anions. The magnetic properties and photocatalytic activity toward the degradation of dyes were investigated. Magnetic susceptibility measurements at 2-300 K for the microcrystals of 1 revealed antiferromagnetic NiⅡ⋯NiⅡ interactions. 1 exhibited excellent photocatalytic capability in the degradation of methyl orange (MO) and rhodamine B (RhB) within 180 min under ultraviolet radiation. The degradation efficiencies reached 83.9% and 71.1% respectively. The mechanism of photocatalytic dye degradation was further discussed.
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