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Citation: Chuan-Tao WANG, Ying-Xian WANG, Li GUO, Zhi-Xiong YANG, Si-Fan ZHOU, Rui DU, Dan-Jun WANG. Construction of Z-scheme CdIn2S4/ZnSnO3 heterostructure for photocatalytic hydrogen production performance[J]. Chinese Journal of Inorganic Chemistry, ;2023, 39(8): 1637-1648. doi: 10.11862/CJIC.2023.127 shu

Construction of Z-scheme CdIn2S4/ZnSnO3 heterostructure for photocatalytic hydrogen production performance

  • Shaanxi Key Laboratory of Chemical Reaction Engineering, College of Chemistry & Chemical Engineering, Yan′an University, Yan′an, Shaanxi 716000, China

  • Corresponding author: Dan-Jun WANG, wangdj761118@163.com
  • Received Date: 7 September 2022
    Revised Date: 15 June 2023

Figures(10)

  • The double shell hollow cube structural ZnSnO3 (ZSO) was prepared by high-temperature calcination with ZnSn(OH)6 as a precursor. Then, the CdIn2S4 (CIS) nanocrystalline was wrapped on the surface of ZSO by a hydrothermal method. Thus CdIn2S4/ZnSnO3 (CIS/ZSO) heterostructures were successfully prepared. The photocatalytic hydrogen evolution reaction (HER) result indicated that the as-prepared 12% CIS/ZSO heterostructure obtained with the molar ratio of CIS to ZSO of 12% exhibited excellent photocatalytic H2-production activity with the hydrogen yield of 1 676.48 μmol·g-1 for 3 h, about 12 times and 8 times of original ZSO and CIS, respectively. The enhanced activity of the ZSO photocatalytic HER was attributed to the successful construction of the CIS/ZSO heterostructure. The formation of the CIS/ZSO heterostructural interface significantly improved the separation efficiency of photogenerated electron/hole pairs and reduced their recombination rate. Furthermore, the possible reaction mechanism was proposed by analyzing the charge transfer pathway.
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