Citation: Xin-Yue XU, Hua-Li CUI, Wen LIU, Xiao-Li CHEN, Hua YANG, Lin LIU, Ji-Jiang WANG. Synthesis and Fluorescence Sensing for Fe³⁺ and p-Nitrophenol of a Copper Coordination Polymer[J]. Chinese Journal of Inorganic Chemistry, ;2022, 38(12): 2539-2549. doi: 10.11862/CJIC.2022.253 shu

Synthesis and Fluorescence Sensing for Fe³⁺ and p-Nitrophenol of a Copper Coordination Polymer

Key Laboratory of New Energy & New Function Materials, Shaanxi Key Laboratory of Chemical Reaction Engineering, College of Chemistry and Chemical Engineering, Yan'an University, Yan'an, Shaanxi 716000, China

Corresponding author: Hua-Li CUI, cuihuali07@163.com
Received Date: 26 July 2022
Revised Date: 9 October 2022

Figures(7)

Under hydrothermal conditions, a coordination polymer {[Cu₂(Hdepa) (2, 2'-bpy)2(H₂O)₂]·2H₂O}_n was designed and synthesized based on ligands H₅depa and 2, 2'-bpy (H₅depa=2, 2', 3, 4', 5-diphenyl ether pentacarboxylic acid, 2, 2'-bpy=2, 2'-bipyridine). Its structure was characterized by elemental analysis, infrared spectroscopy, singlecrystal X-ray diffraction, and thermal stability analysis. The two central Cu²⁺ ions in coordination polymer 1 adopt a five-coordination with triangular bipyramid geometry. The incompletely deprotonated Hdepa^4- ligand adopts a μ₄-η¹-η¹-η¹-η¹ coordination mode. The 2D layers are connected by weak hydrogen bonds to form a 3D supramolecular structure. As a highly sensitive, selective, and multi-response fluorescent sensor, 1 could rapidly detect Fe³⁺ and p-nitrophenol (4-NP). In addition, the fluorescence quenching mechanism was also studied.
- 2, 2', 3, 4', 5-diphenyl ether pentacarboxylic acid,
- hydrothermal method,
- coordination polymer,
- fluorescence sensing
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Synthesis and Fluorescence Sensing for Fe³⁺ and p-Nitrophenol of a Copper Coordination Polymer