Citation: An-Ran WU, Yan-Hui CHEN, Xin-Xin WANG, Wen-Yuan ZHOU, Jia-Wei HE, Jin-Shu WANG, Hong-Yi LI. Pt/TiO₂ Nanotubes Electrode: Preparation by Electroplating Method and Electrocatalytic Hydrogen Evolution Performance[J]. Chinese Journal of Inorganic Chemistry, ;2022, 38(2): 227-236. doi: 10.11862/CJIC.2022.034 shu

Pt/TiO₂ Nanotubes Electrode: Preparation by Electroplating Method and Electrocatalytic Hydrogen Evolution Performance

Faculty of Materials and Manufacturing, Beijing University of Technology, Beijing 100124, China

Corresponding author: Hong-Yi LI, lhy06@bjut.edu.cn
Received Date: 1 April 2021
Revised Date: 14 December 2021

Figures(15)

Here, Pt modified anatase-type titanium dioxide (TiO₂) nanotube arrays were prepared by electroplating method for a low-platinum Pt/TiO₂ nanotubes electrode (Pt/TiO₂-NTs). By contrast, we fixed Pt on TiO₂ dense film by the same procedure as a control sample (Pt/TiO₂-F). The scanning electron microscopy and transmission electron microscopy observation showed that Pt nanoparticles were distributed uniformly in nanotube arrays, and Pt/TiO₂-NTs showed a higher efficiency in electrocatalytic hydrogen evolution compared with Pt/TiO₂-F and commercial Pt/C catalyst, in which the overpotential of Pt/TiO₂-NTs was 0.079 V, the Tafel slope was 42.7 mV·dec^-1 at 10 mA·cm^-2. The catalytic activity of 3 000 cycles duration stability test results showed that Pt/TiO₂-NTs exhibited excellent stability compared with the above contrast electrodes.
- TiO₂ nanotubes carrier,
- electroplating,
- platinum-based catalyst,
- electrocatalytic hydrogen evolution
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Pt/TiO2 Nanotubes Electrode: Preparation by Electroplating Method and Electrocatalytic Hydrogen Evolution Performance

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通讯作者: 陈斌, bchen63@163.com

Pt/TiO₂ Nanotubes Electrode: Preparation by Electroplating Method and Electrocatalytic Hydrogen Evolution Performance