Citation: Lu ZHAO, Tong-Dan CHEN, Han-Ye WANG, Chen-Xi LI, Jiang LI. Mn-Based Coordination Polymer: Facile Synthesis, Structure and Application in Glucose Electrochemical Sensing[J]. Chinese Journal of Inorganic Chemistry, ;2021, 37(11): 2101-2112. doi: 10.11862/CJIC.2021.237 shu

Mn-Based Coordination Polymer: Facile Synthesis, Structure and Application in Glucose Electrochemical Sensing

School of Materials Science and Engineering, Chang'an University, Xi'an 710064, China

Corresponding author: Jiang LI, lijiang@chd.edu.cn
Received Date: 8 June 2021
Revised Date: 31 August 2021

Figures(7)

Utilizing the rigid 6-(3-pyridyl) isophthalic acid (H₂PIAD) linker, one Mn(Ⅱ)-based coordination polymer {[Mn(PIAD)(DMF)]·H₂O}_n (1) was prepared firstly. In order to improve the electrocatalytic activity of glucose sensing, a composite material (Ag@1) was prepared by the strategy of post synthesis of Ag nanoparticles (NPs). The electrocatalytic performance of the glassy carbon electrode (GCE) modified by Ag@1 was evaluated by chronoamperometry method at the optimized application potential, and coordination polymer 1 provided a fixed substrate for the uniform distribution of Ag NPs on its surface. Ag@1 sensor can maximize the electrocatalytic synergistic effect of the combination of Ag and 1 on glucose oxidation. The results reveal that modified GCE by Ag@1 had good performance for the detection of glucose with low detection limit (6.36 μmol·L^-1), good selectivity and sensitivity (166.71 μA·L·mmol^-1·cm^-2).
- manganese,
- coordination polymer,
- Ag nanoparticles,
- glucose sensor
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