Citation: Xi CHEN, Hong-Bo ZHANG, Wen-Tao JIA, Yu-Hang XIA, Chun-Hui SU. Preparation and Luminescence Properties of Tm³⁺-Tb³⁺-Eu³⁺ Co-doped Fluorescence Glass Ceramics Containing Na₃Gd(PO₄)₂[J]. Chinese Journal of Inorganic Chemistry, ;2021, 37(6): 1027-1036. doi: 10.11862/CJIC.2021.115 shu

Preparation and Luminescence Properties of Tm³⁺-Tb³⁺-Eu³⁺ Co-doped Fluorescence Glass Ceramics Containing Na₃Gd(PO₄)₂

School of Material Science and Engineering, Changchun University of Science and Technology, Changchun 130022, China

Corresponding author: Hong-Bo ZHANG, zhb5388460@126.com Chun-Hui SU, sch@cust.edu.cn
Received Date: 27 December 2020
Revised Date: 26 March 2021

Figures(13)

Tm³⁺-Tb³⁺-Eu³⁺ co-doped fluorescence glass ceramics containing Na₃Gd(PO₄)₂ crystals were synthesized by melt crystallization method and luminescence properties were studied. The crystal structure and optimum heat treatment conditions (740℃/3 h) were determined by differential scanning calorimetry (DSC), X-ray diffraction (XRD) and scanning electron microscope (SEM). Under the excitation of 359 nm, when the doping concentrations (molar fraction) of Tm₂O₃, Tb₄O₇ and Eu₂O₃ were 0.2%, 0.2% and 0.95%, respectively, the chromaticity coordinates of glass ceramics were (0.333 2, 0.318 8) close to the standard white light (0.333, 0.333). Combined with fluorescence spectra and fluorescence decay curve analysis, the energy transfer of Tm³⁺→Eu³⁺, Tb³⁺→Eu³⁺ in the sample was confirmed.
- Na₃Gd(PO₄)₂,
- Tm³⁺-Tb³⁺-Eu³⁺,
- glass-ceramic,
- energy transfer,
- luminescence
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沈阳化工大学材料科学与工程学院沈阳 110142

Preparation and Luminescence Properties of Tm3+-Tb3+-Eu3+ Co-doped Fluorescence Glass Ceramics Containing Na3Gd(PO4)2

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通讯作者: 陈斌, bchen63@163.com

Preparation and Luminescence Properties of Tm³⁺-Tb³⁺-Eu³⁺ Co-doped Fluorescence Glass Ceramics Containing Na₃Gd(PO₄)₂