Citation: WEI Yu-Lin, ZHANG Hong-Bo, WANG Tong, ZOU Xiang-Yu, SU Chun-Hui. Synthesis and Energy Transfer of Dy³⁺/Tb³⁺ Co-doped Glass Ceramics Containing SrWO₄ Crystal[J]. Chinese Journal of Inorganic Chemistry, ;2019, 35(12): 2311-2317. doi: 10.11862/CJIC.2019.260 shu

Synthesis and Energy Transfer of Dy³⁺/Tb³⁺ Co-doped Glass Ceramics Containing SrWO₄ Crystal

WEI Yu-Lin ¹ ,
ZHANG Hong-Bo ^1,, ,
WANG Tong ¹ ,
ZOU Xiang-Yu ¹ ,
SU Chun-Hui ^1,2,,

1.
School of Chemistry and Environmental Engineering, Changchun University of Science and Technology, Changchun 130022, China
2.
Changchun Normal University, Changchun 130022, China

Corresponding author: ZHANG Hong-Bo, zhb5388460@126.com SU Chun-Hui, sch@cust.edu.cn
Received Date: 5 July 2019
Revised Date: 18 September 2019

Figures(12)

Dy³⁺/Tb³⁺ co-doped glass ceramics containing SrWO₄ crystal were synthesized successfully by melt-crystallization method and luminescence properties were studied. The optimum heat treatment temperature and time were determined by differential scanning calorimetry (DSC), the precipitation of SrWO₄ grains in the precursor glass was determined by X-ray diffraction (XRD) and combining with the transmittance curves, the optimum heat treatment system was determined at 710℃ for 1.5 h. When the concentration of Dy₂O₃ was 0.8%(n/n), the effect of Tb₄O₇ concentration on the luminescence properties of glass ceramic samples were discussed. It could be seen that with the excitation wavelength 350 nm, there was an obvious peak at 544 nm in the emission spectra of Dy³⁺/Tb³⁺ co-doped glass ceramics. With the increase of Tb₄O₇ concentration, energy transfer efficiency increased gradually, and when the Tb₄O₇ concentration was 1.9%(n/n), the luminescence intensity of green light reached maximum.Basing on the energy transfer theory of Dexter and the decay curves, the energy transfer from Dy³⁺ to Tb³⁺ was determined.
- SrWO₄,
- Dy³⁺/Tb³⁺ co-doped,
- glass ceramics,
- luminescence,
- energy transfer
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Synthesis and Energy Transfer of Dy³⁺/Tb³⁺ Co-doped Glass Ceramics Containing SrWO₄ Crystal