Citation: NIU Yu-Lan, ZHAI Li-Jun, HAO Xiao-Yan, JIA Jiao-Jiao, FAN Li-Ming. Syntheses, Crystal Structures, and Luminescence Sensing of Three Coordination Polymers Based on Bis(benzimidazole) Bridging Linkers[J]. Chinese Journal of Inorganic Chemistry, ;2019, 35(10): 1877-1884. doi: 10.11862/CJIC.2019.217 shu

Syntheses, Crystal Structures, and Luminescence Sensing of Three Coordination Polymers Based on Bis(benzimidazole) Bridging Linkers

1.
Department of Chemistry and Chemical Engineering, Taiyuan Institute of Technology, Taiyuan 030008, China
2.
Department of Chemistry, College of Science, North University of China, Taiyuan 030051, China

Corresponding author: NIU Yu-Lan, niuyulan@163.com FAN Li-Ming, limingfan@nuc.edu.cn
Received Date: 14 June 2019
Revised Date: 21 July 2019

Figures(6)

Three 1D coordination polymers (CPs), namely, {[Mn(bbib)(H₂O)₄](H₂BTC)·2H₂O}_n (1), [Zn(bbib)Cl₂]_n (2), and[Zn(bbibp)Cl₂]_n (3), have been assembled from the reaction of bbib (1, 4-bis(2-benzimidazolyl)benzene) or bbibp (4, 4'-bis(2-benzimidazolyl)biphenyl) and transition metal salts. Their structures have been determined by single-crystal X-ray diffraction analyses and further characterized by elemental analyses (EA), IR spectra, powder X-ray diffraction (PXRD), and thermogravimetric (TG) analyses. Structural analysis reveals that the strong O-H…O hydrogen bonds in 1, and C-H…Cl hydrogen bonds in 2 and 3 play important roles in the formation of those CPs, with the final packing architectures being (4, 6)-connected {4²·5⁸·6⁴·7}{4²·6⁴} net for 1, 5-connected {4³·6⁷} net for 2, and 6-connected (4⁸·6⁷)-msw net for 3. Besides, the luminescent sensing investigation indicates that complexes 2 and 3 exhibit highly sensitivity and selectively sensing of Fe³⁺ ion in aqueous solutions.
- coordination polymers,
- bis(benzimidazo-1-ly) ligand,
- crystal structure,
- luminescent sensing
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