Citation: LI Xin-Shu, WANG Qian, DING Bin. Polymorphic One-and Two-dimensional Zinc(Ⅱ) Coordination Polymers: Hydrothermal Preparation and Recyclable Photoluminescent Sensing for Picric Acid[J]. Chinese Journal of Inorganic Chemistry, ;2019, 35(3): 515-523. doi: 10.11862/CJIC.2019.057 shu

Polymorphic One-and Two-dimensional Zinc(Ⅱ) Coordination Polymers: Hydrothermal Preparation and Recyclable Photoluminescent Sensing for Picric Acid

LI Xin-Shu ^1,2 ,
WANG Qian ^1,2,, ,
DING Bin ^1,2,,

1.
Tianjin Key Laboratory of Structure and Performance for Functional Molecules, MOE Key Laboratory of Inorganic-Organic Hybrid Functional Material Chemistry, College of Chemistry, Tianjin Normal University, Tianjin 300387, China
2.
Key Laboratory of Advanced Energy Materials Chemistry, Ministry of Education, Nankai University, Tianjin 300071, China

Corresponding author: WANG Qian, hxxywq@tjnu.edu.cn DING Bin, hxxydb@mail.tjnu.edu.cn
Received Date: 13 September 2018
Revised Date: 15 December 2018

Figures(7)

A semi-rigid bi-functional multi-dentate ligand 5-(4-((1H-1, 2, 4-triazol-1-yl)methyl)phenyl)-1H-tetrazole (HL) has been employed to prepare two polymorphic zinc(Ⅱ) coordination polymers, namely[Zn(μ₂-L)₂]_n (1) and[Zn(μ₂-L)₂]_n (2) under hydrothermal conditions. Complexes 1 and 2 present temperature induced polymorphic zinc(Ⅱ)-L 1D (1) and 2D (2) coordination frameworks. In 1, 1D left-and right-handed helical chains are inter-linked to form a 1D chain zinc(Ⅱ)-L coordination polymer. In 2, these 1D left-and right-handed helical chains are also interlinked via central zinc(Ⅱ) ions forming the two-dimensional(2D) coordination framework. The photoluminescent properties of free HL and 1~2 have been investigated, indicating strong emissions. Additionally, photoluminescent experiment also demonstrates that complex 2 exhibits highly sensitive luminescence sensing for picric acid in the aqueous solutions with high quenching efficiency (K_SV=3.65×10³ L·mol^-1) and low detection limit (3.004 μmol·L^-1, S/N=3), which make it a promising candidate for sensing picric acid.
- hydrothermal,
- polymorphic,
- zinc,
- photo-luminescence sensing,
- picric acid
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